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1,2,4-Triazoles have proved to be most useful framework for biological activities among nitrogen containing five membered heterocycles. 4-Aryltriazole derivatives have been found to be potent drug which possess a wide spectrum of biological activity. Different types of 1,2,4-triazole derivatives shows variety of pharmacological activities such as antidepressant, anti-inflammatory etc. Considering the increasing importance of compounds bearing 1,2,4-triazole nucleus, Its construction has attracted considerable attention of researchers. The book focuses on main aspects of chemical reaction, mechanism, characterization and applications of synthetic utility. The content is explained in an easy and simple language. It will be a good source of information about fundamental knowledge of organic synthesis of 1,2,4-triazoles as well as reaction path with mechanism to students at undergraduate level, post Graduate level, researchers as well as industrial chemist.