The 33rd Annual Denver Conference on Applications of X-Ray Analysis was held July 30-August 3. 1984. on the campus of the University of Denver. Following the recent tradition of alternating plenary lecture topics between X-ray diffraction and X-ray fluorescence at the confer ence. the plenary sessions dealt with topics of X-ray fluorescence. Prof. H. Aiginger presented a plenary lect~re on TOTAL REFLECTANCE X-RAY SPECTROMETRY which admirably described this relatively new technique. J. C. Russ discussed XRF AND OTHER SURFACE ANALYTICAL TECHNIQUES which gave an excellent overview of the role…mehr
The 33rd Annual Denver Conference on Applications of X-Ray Analysis was held July 30-August 3. 1984. on the campus of the University of Denver. Following the recent tradition of alternating plenary lecture topics between X-ray diffraction and X-ray fluorescence at the confer ence. the plenary sessions dealt with topics of X-ray fluorescence. Prof. H. Aiginger presented a plenary lect~re on TOTAL REFLECTANCE X-RAY SPECTROMETRY which admirably described this relatively new technique. J. C. Russ discussed XRF AND OTHER SURFACE ANALYTICAL TECHNIQUES which gave an excellent overview of the role XRF plays in a modern analytical laboratory. J. E. Taggart. Jr. described THE ROLE OF XRF IN A MODERN GEOCHEMICAL LABORATORY and presented many case histories of the configura tion of analytical equipment in several geochemical laboratories. The plenary lectures demonstrated both the dynamic nature of research in X-ray fluorescence. and the important role X-ray spectrom etry plays in the arsenal of analytical methods found in modern labora tories. Total reflectance X-ray spectrometry takes advantage of con sideration of the geometry of the X-ray optics. Potentially. new sample types may be considered as X-ray fluorescence specimens using this technique.
I. The Role of X-Ray Fluorescence in a Modern Analytical Laboratory (Plenary Session Papers).- Total Reflectance X-Ray Spectrometry.- XRF and Other Surface Analysis Techniques.- The Role of X-Ray Fluorescence in a Modern Geochemical Laboratory.- II. Mathematical Models And Computer Applications In XRF.- Use of Primary Beam Filtration in Estimating Mass Attenuation Coefficients by Compton Scattering.- An Evaluation of Correction Algorithms, Using Theoretically Calculated Intensities.- Monte Carlo Simulations of XRF Intensities in Samples Containing a Dispersed Phase.- Two Easily-Overlooked Sources of Error in XRF Intensity Measurements.- Coordination Analysis by High Resolution X-Ray Spectroscopy.- III. New Techniques and Instrumentation in XRF.- The Application of Tunable Monochromatic Synchrotron Radiation to the Quantitative Determination of Trace Elements.- Energy Dispersive X-Ray Fluorescence Analysis Using Synchroton Radiation.- The Application of Linear Polarized X-Rays after Bragg Reflection for X-Ray Fluorescence Analysis..- Trace Analytical Capabilities of Total-Reflection X-Ray Fluorescence Analysis.- Qualitative Analysis of X-Ray Spectra.- K-Edge X-Ray Fluorescence Analysis for Actinide and Heavy Elements Solution Concentration Measurements.- Excitation and Detection of High Energy Chracteristic X-Rays (20-90 KeV) Using a Novel Radiometric Technique.- An Examination of the Overall Stability of an XRF Spectrometer with Special Reference to Fourier Analysis of Temporal Variation.- Evaluation of the New Generation of Dual-Anode X-Ray Tubes.- Comparison of Various X-Ray Tube Types for XRF Analysis.- IV. Recent Developments in Long-Wavelength Spectroscopy.- Reflection Intensity Dependence on Surface and Wavelength from LiF and EDDT Analyzer Crystals.- A SoftX-Ray Experimental Facility.- Wavelength Dispersing Devices for Soft and Ultrasoft X-Ray Spectrometers.- V. Applications of XRF and XRD to Life Sciences and the Environment.- Feasibility Studies of X-Ray Fluorescence as a Method for the In Vivo Determination of Platinum and Other Heavy Metals.- A Fast, Versatile X-Ray Fluorescence Method for Measuring Tin in Impregnated Wood.- Certification of Reference Materials by Energy-Dispersive X-Ray Fluorescence Spectrometry?.- Evaluating the Variability of Southwestern Ceramics with X-Ray Fluorescence.- An XRF Method for the Analysis of Atmospheric Aerosol and Vehicular Particulate Deposits on Filters.- VI. XRF Applications: Mineralogical, General.- Analysis of River Sediments from the Tigre River (Venezuela) by Radioisotope Excited X-Ray Fluorescence.- Energy-Dispersive XRF Analysis of Intact Salt Drill Cores.- The Use of Rapid Quantitative X-Ray Fluorescence Analysis in Paper Manufacturing and Construction Materials Industry.- Analysis of Diatomaceous Earth by X-Ray Fluorescence Techniques.- Fundamental Parameters vs. Multiple Regression Calculations for the Determination of Europium in Oxide Catalyst Supports by XRF.- EDXRF Determination of Major and Minor Elements in Compound Fertilizers.- Analysis of Wet-Process Phosphoric Acid and By-Product Filter Cake by X-Ray Spectrometry.- VII. New Techniques and Instrumentation in XRD.- The Rapid Simultaneous Measurement of Thermal and Structural Data by a Novel DSC/XRD Instrument.- Balanced Filters for an Annular Counter.- X-Ray Diffraction Measurements via a UNIX+ Based System.- TSX-PLUS Multi-Tasking Upgrade for the Nicolet L-11 Powder Diffraction System.- VIII. X-Ray Strain and Stress Determination.- X-Ray Multiaxial Stress Analysis on Materials with Stress Gradient by Use of Cos? Function.- A Practical ?-Method for the Evaluation of Stress on Materials with Stress Gradient by X-Rays.- Residual Stress Measurements in Inconel Alloy 600 Tubing Using an Advanced X-Ray Instrument and Cr K? Radiation.- Determination of the Unstressed Lattice Parameter "ao" for (Triaxial) Residual Stress Determination by X-Rays.- X-Ray Fractographic Approach to Fracture Toughness of AISI 4340 Steel.- Strain Measurements on Single Crystals and Macrograins with the Aid of an Automated Phi-Psi Goniometer.- IX. XRD Search/Match Methods and Quantitative Analysis.- The Quality of X-Ray Diffraction Standards for Phosphate Minerals and the Degree of Success in Computer Identification.- Results of a Round Robin Study of Systematic Errors Found in Routine X-Ray Diffraction Raw Data.- An X-Ray Diffraction Procedure for Measuring Retained Austenite in High Chromium White Cast Iron.- Quantitative X-Ray Analysis of ICPP Simulated High Alumina Calcine.- X. XRD Applications.- High Temperature XRD Studies of Selected Carbonate Minerals.- High Temperature X-Ray Diffraction Studies of the Defluorination Reactions of Chukhrovite, Falphite and Ralstonite.- Low Thermal Expansion of Alkali Zirconium Phosphates Using a Microcomputer Automated Diffractometer.- The Structure and Lattice Parameters of Pentaerythritol Above and Below Its Phase-Transition Temperature.- A Comparison of Detection Systems for Trace Phase Analysis.- X-Ray Diffraction/Electron Microprobe Analysis of Surface Films Formed on Alloys During Hydrothermal Reaction with Geologic Materials.- Determination of the Crystal System of a Neodymium-Iron-Boron Alloy by X-Ray Diffraction.- An X-Ray Diffraction Method for the Determination of Temperatures in Coke Reactions.- Author Index.
I. The Role of X-Ray Fluorescence in a Modern Analytical Laboratory (Plenary Session Papers).- Total Reflectance X-Ray Spectrometry.- XRF and Other Surface Analysis Techniques.- The Role of X-Ray Fluorescence in a Modern Geochemical Laboratory.- II. Mathematical Models And Computer Applications In XRF.- Use of Primary Beam Filtration in Estimating Mass Attenuation Coefficients by Compton Scattering.- An Evaluation of Correction Algorithms, Using Theoretically Calculated Intensities.- Monte Carlo Simulations of XRF Intensities in Samples Containing a Dispersed Phase.- Two Easily-Overlooked Sources of Error in XRF Intensity Measurements.- Coordination Analysis by High Resolution X-Ray Spectroscopy.- III. New Techniques and Instrumentation in XRF.- The Application of Tunable Monochromatic Synchrotron Radiation to the Quantitative Determination of Trace Elements.- Energy Dispersive X-Ray Fluorescence Analysis Using Synchroton Radiation.- The Application of Linear Polarized X-Rays after Bragg Reflection for X-Ray Fluorescence Analysis..- Trace Analytical Capabilities of Total-Reflection X-Ray Fluorescence Analysis.- Qualitative Analysis of X-Ray Spectra.- K-Edge X-Ray Fluorescence Analysis for Actinide and Heavy Elements Solution Concentration Measurements.- Excitation and Detection of High Energy Chracteristic X-Rays (20-90 KeV) Using a Novel Radiometric Technique.- An Examination of the Overall Stability of an XRF Spectrometer with Special Reference to Fourier Analysis of Temporal Variation.- Evaluation of the New Generation of Dual-Anode X-Ray Tubes.- Comparison of Various X-Ray Tube Types for XRF Analysis.- IV. Recent Developments in Long-Wavelength Spectroscopy.- Reflection Intensity Dependence on Surface and Wavelength from LiF and EDDT Analyzer Crystals.- A SoftX-Ray Experimental Facility.- Wavelength Dispersing Devices for Soft and Ultrasoft X-Ray Spectrometers.- V. Applications of XRF and XRD to Life Sciences and the Environment.- Feasibility Studies of X-Ray Fluorescence as a Method for the In Vivo Determination of Platinum and Other Heavy Metals.- A Fast, Versatile X-Ray Fluorescence Method for Measuring Tin in Impregnated Wood.- Certification of Reference Materials by Energy-Dispersive X-Ray Fluorescence Spectrometry?.- Evaluating the Variability of Southwestern Ceramics with X-Ray Fluorescence.- An XRF Method for the Analysis of Atmospheric Aerosol and Vehicular Particulate Deposits on Filters.- VI. XRF Applications: Mineralogical, General.- Analysis of River Sediments from the Tigre River (Venezuela) by Radioisotope Excited X-Ray Fluorescence.- Energy-Dispersive XRF Analysis of Intact Salt Drill Cores.- The Use of Rapid Quantitative X-Ray Fluorescence Analysis in Paper Manufacturing and Construction Materials Industry.- Analysis of Diatomaceous Earth by X-Ray Fluorescence Techniques.- Fundamental Parameters vs. Multiple Regression Calculations for the Determination of Europium in Oxide Catalyst Supports by XRF.- EDXRF Determination of Major and Minor Elements in Compound Fertilizers.- Analysis of Wet-Process Phosphoric Acid and By-Product Filter Cake by X-Ray Spectrometry.- VII. New Techniques and Instrumentation in XRD.- The Rapid Simultaneous Measurement of Thermal and Structural Data by a Novel DSC/XRD Instrument.- Balanced Filters for an Annular Counter.- X-Ray Diffraction Measurements via a UNIX+ Based System.- TSX-PLUS Multi-Tasking Upgrade for the Nicolet L-11 Powder Diffraction System.- VIII. X-Ray Strain and Stress Determination.- X-Ray Multiaxial Stress Analysis on Materials with Stress Gradient by Use of Cos? Function.- A Practical ?-Method for the Evaluation of Stress on Materials with Stress Gradient by X-Rays.- Residual Stress Measurements in Inconel Alloy 600 Tubing Using an Advanced X-Ray Instrument and Cr K? Radiation.- Determination of the Unstressed Lattice Parameter "ao" for (Triaxial) Residual Stress Determination by X-Rays.- X-Ray Fractographic Approach to Fracture Toughness of AISI 4340 Steel.- Strain Measurements on Single Crystals and Macrograins with the Aid of an Automated Phi-Psi Goniometer.- IX. XRD Search/Match Methods and Quantitative Analysis.- The Quality of X-Ray Diffraction Standards for Phosphate Minerals and the Degree of Success in Computer Identification.- Results of a Round Robin Study of Systematic Errors Found in Routine X-Ray Diffraction Raw Data.- An X-Ray Diffraction Procedure for Measuring Retained Austenite in High Chromium White Cast Iron.- Quantitative X-Ray Analysis of ICPP Simulated High Alumina Calcine.- X. XRD Applications.- High Temperature XRD Studies of Selected Carbonate Minerals.- High Temperature X-Ray Diffraction Studies of the Defluorination Reactions of Chukhrovite, Falphite and Ralstonite.- Low Thermal Expansion of Alkali Zirconium Phosphates Using a Microcomputer Automated Diffractometer.- The Structure and Lattice Parameters of Pentaerythritol Above and Below Its Phase-Transition Temperature.- A Comparison of Detection Systems for Trace Phase Analysis.- X-Ray Diffraction/Electron Microprobe Analysis of Surface Films Formed on Alloys During Hydrothermal Reaction with Geologic Materials.- Determination of the Crystal System of a Neodymium-Iron-Boron Alloy by X-Ray Diffraction.- An X-Ray Diffraction Method for the Determination of Temperatures in Coke Reactions.- Author Index.
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