In this book, the proceedings of the Third European Symposium on "Analysis of Organic Micropollutants in Water", held in Oslo (Norway), from 19 to 21 September 1983, are presented. The symposium was organized within the framework of the Concerted Ac tion COST 64b bis _, which has the same name and is included in the Third R&D Programme on Environment of the Commission of the European Communi ties - Indirect and Concerted Actions - 1981 to 1985. The aim of the symposium was to review the progress and results achiev ed during the past two years, since the Second symposium, held in Killarney…mehr
In this book, the proceedings of the Third European Symposium on "Analysis of Organic Micropollutants in Water", held in Oslo (Norway), from 19 to 21 September 1983, are presented. The symposium was organized within the framework of the Concerted Ac tion COST 64b bis _, which has the same name and is included in the Third R&D Programme on Environment of the Commission of the European Communi ties - Indirect and Concerted Actions - 1981 to 1985. The aim of the symposium was to review the progress and results achiev ed during the past two years, since the Second symposium, held in Killarney (Ireland) in November 1981. The programme of the symposium consisted of review papers covering dif ferent areas related to the analysis of the organic pollutants in water, in cluding sampling and sample treatment, gas and liquid chromatography, mass spectrometry and specific analytical problems for some types of compounds. We think that the volume gives a rather complete overview of these activities in Europe. Moreover, the paper presented by D. Hunt reviews the development of the new technique mass spectrometry - mass spectrometry in the United States of America. Some special sessions concerned the presentation of original contri butions in form of poster, the extended versions of which are published in this volume.
Session I - Sampling.- Introductory remarks on sampling.- Zur Entnahme von Grundwasserproben.- Sampling of surface waters for tracing macro- and micro-pollutants.- Techniques d' e´chantillonnage pour 1' analyse des traces organiques.- Extraction of sediments using ultrasonic and steam distillation treatments.- Session II-Analysis.- High resolution gas chromatography in water analysis: 12 years of development.- Analysis of organics in the environment by functional group using a triple quadrupole mass spectrometer.- Recent progress in LC/MS.- Computerized data handling in gas chranatography/mass spectrometry.- New developments in selective detection in capillary gas chromatography.- Determination of organic water pollutants by the combined use of high-performance liquid chromatography and high-resolution gas chromatography.- Analysis of organic micropollutants by HPLC.- Identification of non-volatile organics in water using field desorption mass spectrometry and high performance liquid chromatography.- Mass spectrometric identification of surfactants.- Characterisation of non-volatile organics from water by pyrolysis-gaschromatography-mass spectrometry.- Automated GC/MS for analysis of aromatic hydrocarbons in the marine environment.- Analysis of sulphonic acids and other ionic organic compounds using reversed-phase HPLC.- Closed loop stripping and cryogenic on-column focusing of trihalomethanes and related compounds for capillary gas chromatography.- Observations with cold on-column injection.- Polymethylphenylsilicones in fused silica capillary columns for gas chromatography.- Collaborative study on the mass spectrometric quantitative determination of toluene using isotope dilution technique.- Determination of volatile organic substances in water by GC/SIM resultsof an investigation on the rivers Rhine and Main.- Session III-Specific Analytical Problems.- Analytische Bestimmung organischer Halogenverbindungen.- Determination of organic sulphur, organic phosphorus and organic nitrogen.- Results from Round Robin Exercises of phenolic compounds within the COST 64b bis project.- Instrumental analysis of petroleum hydrocarbons.- Screening of pollution from a former municipal waste dump at the bank of a Danish inlet.- The impact on the ecology of polychlorinated phenols and other organics dumped at the bank of a small marine inlet.- Organic micropollutants from the pulp industry: analysis of lake Päijänne water.- Ground water pollution by organic solvents and their microbial degradation products.- Comparison of three methods for organic halogen determination in industrial effluents.- Organic micropollutants in surface waters of the Glatt Valley, Switzerland.- Species and persistence of pollutants in the pond water from an orchard area treated with organophosphorus pesticides.- Occurrence and origin of brominated phenols in Barcelona's water supply.- The relationship between the concentration of organic matter in natural waters and the production of lipophilic volatile organohalogen compounds during their chlorination.- Session IV-Future Environmental Problems.- Standard setting principles.- Integration of the environment research action programme into the framework programme for community scientific and technical activities 1984-1987.- COST 64b bis project - Now and the future.- List of Participants.- Index of Authors.
Session I - Sampling.- Introductory remarks on sampling.- Zur Entnahme von Grundwasserproben.- Sampling of surface waters for tracing macro- and micro-pollutants.- Techniques d' e´chantillonnage pour 1' analyse des traces organiques.- Extraction of sediments using ultrasonic and steam distillation treatments.- Session II-Analysis.- High resolution gas chromatography in water analysis: 12 years of development.- Analysis of organics in the environment by functional group using a triple quadrupole mass spectrometer.- Recent progress in LC/MS.- Computerized data handling in gas chranatography/mass spectrometry.- New developments in selective detection in capillary gas chromatography.- Determination of organic water pollutants by the combined use of high-performance liquid chromatography and high-resolution gas chromatography.- Analysis of organic micropollutants by HPLC.- Identification of non-volatile organics in water using field desorption mass spectrometry and high performance liquid chromatography.- Mass spectrometric identification of surfactants.- Characterisation of non-volatile organics from water by pyrolysis-gaschromatography-mass spectrometry.- Automated GC/MS for analysis of aromatic hydrocarbons in the marine environment.- Analysis of sulphonic acids and other ionic organic compounds using reversed-phase HPLC.- Closed loop stripping and cryogenic on-column focusing of trihalomethanes and related compounds for capillary gas chromatography.- Observations with cold on-column injection.- Polymethylphenylsilicones in fused silica capillary columns for gas chromatography.- Collaborative study on the mass spectrometric quantitative determination of toluene using isotope dilution technique.- Determination of volatile organic substances in water by GC/SIM resultsof an investigation on the rivers Rhine and Main.- Session III-Specific Analytical Problems.- Analytische Bestimmung organischer Halogenverbindungen.- Determination of organic sulphur, organic phosphorus and organic nitrogen.- Results from Round Robin Exercises of phenolic compounds within the COST 64b bis project.- Instrumental analysis of petroleum hydrocarbons.- Screening of pollution from a former municipal waste dump at the bank of a Danish inlet.- The impact on the ecology of polychlorinated phenols and other organics dumped at the bank of a small marine inlet.- Organic micropollutants from the pulp industry: analysis of lake Päijänne water.- Ground water pollution by organic solvents and their microbial degradation products.- Comparison of three methods for organic halogen determination in industrial effluents.- Organic micropollutants in surface waters of the Glatt Valley, Switzerland.- Species and persistence of pollutants in the pond water from an orchard area treated with organophosphorus pesticides.- Occurrence and origin of brominated phenols in Barcelona's water supply.- The relationship between the concentration of organic matter in natural waters and the production of lipophilic volatile organohalogen compounds during their chlorination.- Session IV-Future Environmental Problems.- Standard setting principles.- Integration of the environment research action programme into the framework programme for community scientific and technical activities 1984-1987.- COST 64b bis project - Now and the future.- List of Participants.- Index of Authors.
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