Carbohydrate Chemistry
Proven Synthetic Methods, Volume 2
Herausgeber: Marel, Gijsbert van der; Codee, Jeroen
Carbohydrate Chemistry
Proven Synthetic Methods, Volume 2
Herausgeber: Marel, Gijsbert van der; Codee, Jeroen
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This second volume in a series offers a collection of synthetic procedures valuable to the practice of synthetic carbohydrate chemistry, both for specific synthetic transformations and the preparation of common synthetic intermediates. Each chapter presents in-depth experimental descriptions for the reported procedures, including reaction setup, reaction conditions, work-up procedures, and purification protocols. All described procedures have been independently verified as reliable and reproducible. With editors and contributors who are highly respected scientists in the field, this book…mehr
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- Produktdetails
- Verlag: CRC Press
- Seitenzahl: 334
- Erscheinungstermin: 4. März 2014
- Englisch
- Abmessung: 240mm x 161mm x 23mm
- Gewicht: 666g
- ISBN-13: 9781439875940
- ISBN-10: 1439875944
- Artikelnr.: 34376874
- Herstellerkennzeichnung
- Produktsicherheitsverantwortliche/r
- Europaallee 1
- 36244 Bad Hersfeld
- gpsr@libri.de
- Verlag: CRC Press
- Seitenzahl: 334
- Erscheinungstermin: 4. März 2014
- Englisch
- Abmessung: 240mm x 161mm x 23mm
- Gewicht: 666g
- ISBN-13: 9781439875940
- ISBN-10: 1439875944
- Artikelnr.: 34376874
- Herstellerkennzeichnung
- Produktsicherheitsverantwortliche/r
- Europaallee 1
- 36244 Bad Hersfeld
- gpsr@libri.de
-d-glucopyranosyl)prop-2-ene. Synthesis of a Multivalent Glycocyclopeptide Using Oxime Ligation. Reductive Amination Methodology for Synthesis of Primary Amines from Unprotected Synthons. General Preparation of Imidazole-1-sulfonate Esters. Regioselective Monoacylation and Monoalkylation of Carbohydrates Catalyzed by a Diarylborinic Ester. The Synthesis of Carbamates from Alkenylamines. Hydrolysis of Thioglycosides Using Anhydrous N-Iodosuccinimide (NIS) and Trifluoroacetic Acid (TFA). Highly Diastereoselective Construction of l-Heptosides by a Sequential Grignard Addition/Fleming-Tamao Oxidation. Synthesis of Fluorinated Exo- glycals Mediated by Selectfluor. A Direct and Stereospecific Approach to the Synthesis of
-Glycosyl Thiols. Efficient Microwave-Assisted Synthesis of 1
,2,3,3
,4,4
,6-Hepta-O-benzyl-sucrose and 1
,2,3,3
,4,4
-Hexa-O -benzylsucrose. Section II: Synthetic Intermediates. Oligosaccharide-Salicylaldehyde Derivatives as Precursors of Water-Soluble, Biocompatible Anion Receptors. Allyl 3,4,6-Tri-O -Benzyl-
-d-Mannopyranoside. Synthesis of a Spacer-Armed 6
-Sialyl-N -Acetyllactosamine. Synthesis of ß-(1
3)-mannobiose. Phenyl 4,6-O -Benzylidene-1-thio-
-d-mannopyranoside. Synthesis of 1,3,4,6-Tetra-O-acetyl-
-d-glucopyranose Revisited. Synthesis of 4,6-O -Benzylidene Acetals of Methyl
-d-Glucopyranoside, Ethyl 1-Thio-ß-d-gluco- and Galactopyranoside. Synthesis of
-N-Acetylneuraminic Acid Methyl Glycoside. Synthesis of Ammonium 3-Deoxy-d-manno-oct-2-ulopyranosylonate (Ammonium Kdo). Synthesis and Characterization of Tetra-O-propargyl Pentaerythritol. Improved Synthesis of Ethyl (2,3,4,6-Tetra-O- acetyl-ß-d-galactopyranosyl)-(1
3)-4,6-O -benzylidene-2-deoxy-1-thio-2-trichloroacetamido-ß-d-glucopyranoside. Synthesis of
-d-Galactofuranosyl Phosphate. Synthesis of 1,2 4,5-Di-O -(3,3-pentylidene)arabitol via Kinetic Acetal Formation. 1,2-Anhydro-3,4,6-tri-O-benzyl-ß-d-mannopyranose. Synthesis of Glucosyl C-1 Dihalides from Tetra-O-acetyl-ß-d-glucopyranosyl Chloride. Synthesis of 3,4,6-Tri-O-acetyl-d-galactal. Efficient Synthesis of Hepta-O -acetyl-ß-lactosyl Azide via Phase Transfer Catalysis. Synthesis of 2,3,4,6-Tetra-O-acetyl-
-d-mannopyranosyl Azide. Synthesis of Phenyl 2,3,4,6-Tetra-O-acetyl-1-thio-ß-d-galactopyranoside. An Alternative, Large-Scale Synthesis of 1,2 5,6-Di-O-isopropylidene-
-d-ribo -hex-3-ulofuranose.
-d-glucopyranosyl)prop-2-ene. Synthesis of a Multivalent Glycocyclopeptide Using Oxime Ligation. Reductive Amination Methodology for Synthesis of Primary Amines from Unprotected Synthons. General Preparation of Imidazole-1-sulfonate Esters. Regioselective Monoacylation and Monoalkylation of Carbohydrates Catalyzed by a Diarylborinic Ester. The Synthesis of Carbamates from Alkenylamines. Hydrolysis of Thioglycosides Using Anhydrous N-Iodosuccinimide (NIS) and Trifluoroacetic Acid (TFA). Highly Diastereoselective Construction of l-Heptosides by a Sequential Grignard Addition/Fleming-Tamao Oxidation. Synthesis of Fluorinated Exo- glycals Mediated by Selectfluor. A Direct and Stereospecific Approach to the Synthesis of
-Glycosyl Thiols. Efficient Microwave-Assisted Synthesis of 1
,2,3,3
,4,4
,6-Hepta-O-benzyl-sucrose and 1
,2,3,3
,4,4
-Hexa-O -benzylsucrose. Section II: Synthetic Intermediates. Oligosaccharide-Salicylaldehyde Derivatives as Precursors of Water-Soluble, Biocompatible Anion Receptors. Allyl 3,4,6-Tri-O -Benzyl-
-d-Mannopyranoside. Synthesis of a Spacer-Armed 6
-Sialyl-N -Acetyllactosamine. Synthesis of ß-(1
3)-mannobiose. Phenyl 4,6-O -Benzylidene-1-thio-
-d-mannopyranoside. Synthesis of 1,3,4,6-Tetra-O-acetyl-
-d-glucopyranose Revisited. Synthesis of 4,6-O -Benzylidene Acetals of Methyl
-d-Glucopyranoside, Ethyl 1-Thio-ß-d-gluco- and Galactopyranoside. Synthesis of
-N-Acetylneuraminic Acid Methyl Glycoside. Synthesis of Ammonium 3-Deoxy-d-manno-oct-2-ulopyranosylonate (Ammonium Kdo). Synthesis and Characterization of Tetra-O-propargyl Pentaerythritol. Improved Synthesis of Ethyl (2,3,4,6-Tetra-O- acetyl-ß-d-galactopyranosyl)-(1
3)-4,6-O -benzylidene-2-deoxy-1-thio-2-trichloroacetamido-ß-d-glucopyranoside. Synthesis of
-d-Galactofuranosyl Phosphate. Synthesis of 1,2 4,5-Di-O -(3,3-pentylidene)arabitol via Kinetic Acetal Formation. 1,2-Anhydro-3,4,6-tri-O-benzyl-ß-d-mannopyranose. Synthesis of Glucosyl C-1 Dihalides from Tetra-O-acetyl-ß-d-glucopyranosyl Chloride. Synthesis of 3,4,6-Tri-O-acetyl-d-galactal. Efficient Synthesis of Hepta-O -acetyl-ß-lactosyl Azide via Phase Transfer Catalysis. Synthesis of 2,3,4,6-Tetra-O-acetyl-
-d-mannopyranosyl Azide. Synthesis of Phenyl 2,3,4,6-Tetra-O-acetyl-1-thio-ß-d-galactopyranoside. An Alternative, Large-Scale Synthesis of 1,2 5,6-Di-O-isopropylidene-
-d-ribo -hex-3-ulofuranose.