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The objective of this book is to provide useful information to researchers who are interested in the field of CNTs for electroanalysis. Five different parameters have been studied for the suitability of CNTs for electroanalysis. The five parameters are concentration of PVA, concentration of CNTs, pH values and concentration of surfactants such as SDS and HDTAB. Characterisation of CNTs was done by using scanning electron microscopy, Raman spectroscopy and potentiostat/galvanostat station.