Micro process engineering is approaching both academia and industry. With the provision of micro devices and systems by commercial suppliers, one main barrier for using these units has been eliminated. This book focuses on processes rather than on devices: what is 'before' and 'behind' micro device fabrication - and gives a comprehensive and detailed overview on A multi-faceted, hierarchic analysis of chemical micro process technology - Modelling and simulation of micro reactors - Liquid- and liquid/liquid-phase reactions - Gas/liquid reactions - Gas-phase reactions (heterogeneous catalysis)
Micro process engineering is approaching both academia and industry. With the provision of micro devices and systems by commercial suppliers, one main barrier for using these units has been eliminated. This book focuses on processes rather than on devices: what is 'before' and 'behind' micro device fabrication - and gives a comprehensive and detailed overview on A multi-faceted, hierarchic analysis of chemical micro process technology - Modelling and simulation of micro reactors - Liquid- and liquid/liquid-phase reactions - Gas/liquid reactions - Gas-phase reactions (heterogeneous catalysis)
Volker Hessel, born 1964, was appointed Vice Director R&D and Head of the Chemical Process Technology Department at the Institut für Mikrotechnik Mainz GmbH (IMM) in 2002. His department focuses on mixing, fine chemistry, and energy generation by fuel processing using microstructured reactors. He obtained his Ph.D. from the University of Mainz on organic chemistry in 1993, investigating structure-property relations of supramolecular structures. After having been appointed Group Leader for Microreaction Technology at the IMM in 1996, he became Head of the newly founded Department of Microreaction Technology in 1999. He is author of more than 90 peer-reviewed publications in the field of organic chemistry and chemical micro process engineering, 200 papers in total, 3 books and 15 patents.
Holger Löwe, born in 1953, was appointed as Professor for Chemical Micro Process Technology at the Chemistry, Pharmaceutics and Earth Sciences Department of the Johannes Gutenberg University Mainz in 2005. He studied chemistry at the University of Leipzig and obtained his Ph.D. on alkylation of phenols in 1984 after working as Research Group Leader at the Filmfabrik Wolffen from 1977 to 1984. The same year, he moved to the Faculty of Electrochemistry at the Technical University in Ilmenau, where he was Head of the Chemistry Section at the internal college. He joined the IMM in 1991. After becoming Leader of the Electrochemistry Group and subsequently, Head of theChemistry/Microreaction Technology Department, he was appointed Director of R&D in 1999. He is author of more than 280 publications and 30 patents.
Inhaltsangabe
From the contents: A MULTI-FACETED, HIERARCHIC ANALYSIS OF CHEMICAL MICRO PROCESS TECHNOLOGY. Micro Reactor Differentiation and Process Intensification. Consequences of Chemical Micro Processing. Physical and Chemical Implications. Impact on Chemical Engineering. Impact on Process Engineering. Impact on Process Results. Impact on Society and Ecology. Impact on Economy. Application Fields and Markets of Micro Reactors. MODELLING AND SIMULATION OF MICRO REACTORS. Flow Phenomena on the Microscale. Methods of Computational Fluid Dynamics. Flow Distributions. Heat Transfer. Mass Transfer and Mixing. Reaction Kinetics and Modelling. Free Surface Flow. Flow in Porous Media. GAS-PHASE REACTIONS. Catalyst Coatings in Micro Channels. Micro Reactors for Gas-Phase Reactions. Oxidations. Hydrogenations. Dehydrogenations. Substitutions. Eliminations. Additions and Coupling Reactions. LIQUID- AND LIQUID/LIQUID-PHASE REACTIONS. Micro Reactors for Liquid-Phase and Liquid/Liquid-Phase Reactions. Aliphatic Nucleophilic and Electrophilic Substitution such as Esterification, Acylation of Amines, Thiocyanation a. m. m. Aromatic Electrophilic and Nucleophilic Substitution such as Nitrations, Amino-de-halogenations, Diazo Chemistry a. m. m. Metal-catalyzed Aromatic Substitution such as Suzuki and Sonogashira Couplings a. m. Free Radical Substitution such as Alkane Nitration. Addition to Carbon-Carbon and Carbon-hetero Multiple Bonds such as the Michael Addition, the Diels-Alder-Reaction, the Aldol Reaction a. m. m. Oxidations and Reductions. Eliminations and Rearrangements. Inorganic Reactions such as the Belousov-Zhabotinskii-Reaction, Complex Formations a. m. m. GAS/LIQUID CONTACTING. Micro Reactors for Gas/Liquid Contacting. Aromatic Electrophilic Substitution such as Direct Fluorinations. Free Radical Substitution such as Alkane Fluorinations and Chlorinations. Addition to Carbon-Carbon and Carbon-hetero Multiple Bonds such as Nitro-group Hydrogenation, Cycloalkane Hydrogenation a. m. Oxidations and Reductions such as Alcohol Oxidation, Photo Diels-Alder Reactions a. m. Inorganic Reactions such as Sulfite Oxidation
From the contents: A MULTI-FACETED, HIERARCHIC ANALYSIS OF CHEMICAL MICRO PROCESS TECHNOLOGY. Micro Reactor Differentiation and Process Intensification. Consequences of Chemical Micro Processing. Physical and Chemical Implications. Impact on Chemical Engineering. Impact on Process Engineering. Impact on Process Results. Impact on Society and Ecology. Impact on Economy. Application Fields and Markets of Micro Reactors. MODELLING AND SIMULATION OF MICRO REACTORS. Flow Phenomena on the Microscale. Methods of Computational Fluid Dynamics. Flow Distributions. Heat Transfer. Mass Transfer and Mixing. Reaction Kinetics and Modelling. Free Surface Flow. Flow in Porous Media. GAS-PHASE REACTIONS. Catalyst Coatings in Micro Channels. Micro Reactors for Gas-Phase Reactions. Oxidations. Hydrogenations. Dehydrogenations. Substitutions. Eliminations. Additions and Coupling Reactions. LIQUID- AND LIQUID/LIQUID-PHASE REACTIONS. Micro Reactors for Liquid-Phase and Liquid/Liquid-Phase Reactions. Aliphatic Nucleophilic and Electrophilic Substitution such as Esterification, Acylation of Amines, Thiocyanation a. m. m. Aromatic Electrophilic and Nucleophilic Substitution such as Nitrations, Amino-de-halogenations, Diazo Chemistry a. m. m. Metal-catalyzed Aromatic Substitution such as Suzuki and Sonogashira Couplings a. m. Free Radical Substitution such as Alkane Nitration. Addition to Carbon-Carbon and Carbon-hetero Multiple Bonds such as the Michael Addition, the Diels-Alder-Reaction, the Aldol Reaction a. m. m. Oxidations and Reductions. Eliminations and Rearrangements. Inorganic Reactions such as the Belousov-Zhabotinskii-Reaction, Complex Formations a. m. m. GAS/LIQUID CONTACTING. Micro Reactors for Gas/Liquid Contacting. Aromatic Electrophilic Substitution such as Direct Fluorinations. Free Radical Substitution such as Alkane Fluorinations and Chlorinations. Addition to Carbon-Carbon and Carbon-hetero Multiple Bonds such as Nitro-group Hydrogenation, Cycloalkane Hydrogenation a. m. Oxidations and Reductions such as Alcohol Oxidation, Photo Diels-Alder Reactions a. m. Inorganic Reactions such as Sulfite Oxidation
Rezensionen
"Dr. Hessel zählt zu den drei internationalen Top-Experten auf diesem Gebiet.' (Ronald S. Besser, Louisiana Tech University, USA)" ... Mir ist kein Buch mit so starker Ausrichtung in Ingenieurbereiche bekannt. Alle Autoren sind international angesehen für ihre Arbeiten ..." (S.J. Haswell, University of Hull, UK)
"Die Autoren sind führend auf diesem Gebiet und haben einen hervorragenden internationalen Ruf." (Dr. Handa, BP Chemicals, UK)
"Das Renommee der Autoren ist sehr hoch, sie sind führend auf dem Gebiet der Mikrotechnologie." (Dr. Bayer, Siemens Axiva, Frankfurt am Main, Deutschland)
"Die Autoren sind anerkannte und kompetente Fachleute auf dem Gebiet der Mikrotechnologie." (Prof. Hönicke, TU Chemnitz, Deutschland)
"Die kritische Beurteilung der derzeit bekannten Mikroprozesse, die ausführliche Analyse von Literaturdaten und die zahlreichen Literaturhinweise machen Chemical Micro Process Engineering zu einem regelrechten Handbuch der chemischen Mikrotechnologie, das Wissenschaftlern aller Colour als wertvolle Informationsquelle dienen kann." (Claude de Bellefon, Laboratory de Génie des Procédés Catalytiques, CNRS ESCPE Lyon, Villeurbanne, Angewandte Chemie, Dezember 2004)
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