Laborhandbuch und Nachschlagewerk zugleich! Prinzipien, Ausrüstung und technische Details der wichtigsten Trennverfahren werden aus der Sicht der praktischen Anwendung beschrieben, wobei der Autor mit einem Minimum an mathematischen Formeln auskommt. Anhand von 59 Beispielexperimenten wird das richtige Vorgehen demonstriert. Mit diesem Buch lernen auch Anfänger auf dem Gebiet der chemischen Analytik, mit Hilfe kommerzieller Produkte und bewährter Verfahren exakte Ergebnisse zu erzielen. (04/00)
Laborhandbuch und Nachschlagewerk zugleich! Prinzipien, Ausrüstung und technische Details der wichtigsten Trennverfahren werden aus der Sicht der praktischen Anwendung beschrieben, wobei der Autor mit einem Minimum an mathematischen Formeln auskommt. Anhand von 59 Beispielexperimenten wird das richtige Vorgehen demonstriert. Mit diesem Buch lernen auch Anfänger auf dem Gebiet der chemischen Analytik, mit Hilfe kommerzieller Produkte und bewährter Verfahren exakte Ergebnisse zu erzielen. (04/00)
CLIFTON E. MELOAN, phd, is Professor Emeritus of Analytical Chemistry at Kansas State University, Manhattan, Kansas. Extensively published in the field, Dr. Meloan has served as a science advisor to the FDA for nearly 30 years.
Inhaltsangabe
SEPARATIONS INVOLVING PHASE CHANGES. Volatilization. Zone Melting. Distillation: General Information. Azeotropic and Extractive Distillations. Steam and Immiscible Solvents Distillation. Vacuum Distillation. Molecular Distillation and Sublimation. Lyophilization (Freeze Drying). SEPARATIONS INVOLVING EXTRACTION. Extraction: General Concepts. Continuous Extraction. Countercurrent (Extraction) Chromatography: The Ito Coil-Planet Centrifugal Extractor. Solid Phase Extraction. Supercritical Fluid Extraction. SEPARATIONS INVOLVING CHROMATOGRAPHY. Chromatography: General Theory. Displacement and Multiple Column Partition Chromatography. Affinity Chromatography. Size Exclusion Chromatography (Gel Filtration; Gel Permeation). Flash Chromatography. High Performance Liquid Chromatography (HPLC). Gas-Liquid Chromatography. Paper Chromatography. Thin Layer Chromatography. SEPARATIONS INVOLVING ION EXCHANGE RESINS. Ion Exchange. Ion Chromatography. Ion Retardation, Ion Exclusion, and Ligand Exchange. SEPARATIONS INVOLVING ELECTRIC FIELDS. Electrodeposition. Electrophoresis--General. Immunoelectrophoresis. Polyacrylamide Gel Disc Electrophoresis. Ion Focusing, SDS, and Two-Dimensional Electrophoresis. Capillary Zone Electrophoresis. Field Flow Fractionation. SEPARATIONS INVOLVING FLOTATION. Purge and Trap and Dynamic Headspace Analysis Foam Fractionation, Gas-, and Liquid-Assisted Flotation. SEPARATIONS INVOLVING MEMBRANES. Osmosis and Reverse Osmosis. Dialysis and Electrodialysis Filtering and Sieving. SEPARATIONS INVOLVING MISCELLANEOUS TECHNIQUES. Density Gradients. Centrifugation. Masking and Sequestering Agents. Solubility. Gas Analysis by Portable Orsat. Appendices. Index.
SEPARATIONS INVOLVING PHASE CHANGES. Volatilization. Zone Melting. Distillation: General Information. Azeotropic and Extractive Distillations. Steam and Immiscible Solvents Distillation. Vacuum Distillation. Molecular Distillation and Sublimation. Lyophilization (Freeze Drying). SEPARATIONS INVOLVING EXTRACTION. Extraction: General Concepts. Continuous Extraction. Countercurrent (Extraction) Chromatography: The Ito Coil-Planet Centrifugal Extractor. Solid Phase Extraction. Supercritical Fluid Extraction. SEPARATIONS INVOLVING CHROMATOGRAPHY. Chromatography: General Theory. Displacement and Multiple Column Partition Chromatography. Affinity Chromatography. Size Exclusion Chromatography (Gel Filtration; Gel Permeation). Flash Chromatography. High Performance Liquid Chromatography (HPLC). Gas-Liquid Chromatography. Paper Chromatography. Thin Layer Chromatography. SEPARATIONS INVOLVING ION EXCHANGE RESINS. Ion Exchange. Ion Chromatography. Ion Retardation, Ion Exclusion, and Ligand Exchange. SEPARATIONS INVOLVING ELECTRIC FIELDS. Electrodeposition. Electrophoresis--General. Immunoelectrophoresis. Polyacrylamide Gel Disc Electrophoresis. Ion Focusing, SDS, and Two-Dimensional Electrophoresis. Capillary Zone Electrophoresis. Field Flow Fractionation. SEPARATIONS INVOLVING FLOTATION. Purge and Trap and Dynamic Headspace Analysis Foam Fractionation, Gas-, and Liquid-Assisted Flotation. SEPARATIONS INVOLVING MEMBRANES. Osmosis and Reverse Osmosis. Dialysis and Electrodialysis Filtering and Sieving. SEPARATIONS INVOLVING MISCELLANEOUS TECHNIQUES. Density Gradients. Centrifugation. Masking and Sequestering Agents. Solubility. Gas Analysis by Portable Orsat. Appendices. Index.
Rezensionen
"...the book provides a good balance between techniques relevant for chemical separation and experimental work." (The Analyst, 18th August 2000)
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