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Management of technological processes of the rare metals production refers to quite complex technical control systems in which the maintenance of technological regimes within specified limits, monitoring their state requires the collection of a large amount of information and installation of a significant number of instrumentation and operational control. Therefore, there is a need to automate the production of rare metals and create optimal control systems for such processes. The work is devoted to the research and creation of scientific foundations and approaches to the control systems of technological processes for the production of rare metals, the optimization of the extraction technologies in metallurgical production due to the integrated industrial automation of technological processes. Also in the monograph questions of the analysis and development of effective control systems of processes with the increased potential of robust stability in the presence of uncertainties of technological parameters are considered within an industrial automation.