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This book explores the use of electronic microscopes and spectroscopic techniques to solve different problems. Delve into the intricate details of these powerful tools as they reveal some of the hidden mysteries of the microscopic realm. From exploring the inner workings of cells to analyzing the composition of materials at the atomic level, this book offers an engaging and motivating journey into the realm of cutting-edge scientific exploration in electron microscopy and spectroscopy techniques with emerging trends in the field. Whether you are an experienced researcher or a curious enthusiast, this book will motivate your scientific thinking to discover and expand your understanding of the microscopic world, inviting you to continue working in these areas to obtain more interesting results.