The technique described in this book are arranged with regard to present techniques used in material science for experimental methods, to provide an enabling reveal for an extensive areas of researchers as well as industrial. This book, based on describes the value of experiment technique in industrial area for accelerated growth and view. Crystallization, Alum, Thin layer chromatography separation, identification and determination of Rf value,Separation of amino acids by TLC, spectrophotometer, complexometry, iron and chromium from stainless steel, Nephlometric, Orificemeter, Reynold's Number, Bernoulli's Theorem, stalgmometer, viscometer, Cu and Ni by TLC, hardness of water, capacity of ion-exchange resin, U-Tube manometer, stalgmometer using drop weight method.