This book concern Electrochemical Deposition of copper from dilute solutions using packed bed electrode.The aim of work is to investigate the electrodeposition of copper in a fixed packed-bed electrode, in a circulated-batch system, in order to disclose the effects of the following operation parameters on the removal of copper from simulated waste water laden with copper. These parameters are: 1- Time of electrolysis. 2- Initial concentration of copper in simulated waste water. 3- Applied superficial current density. 4- Type and concentration of supporting electrolyte. 5- Flow rate of treated solution. This will provide the opportunity to perform some sort of comparison between packed and fluidized beds. 6- The shape of current collector. After performing the experimental part, attention is directed towards the assessment of the kinetics of electrodeposition process of copper. Finally, a simple economic study is carried out to reveal the cost indicators of the removal process.