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This book has been designed to facilitate the students to build their concept about the fundamentals of experimental chemistry. The basic concept regarding the understanding of solution preparation and dilutions are well explained, graspable even by the beginners of chemistry. The student have also been introduced to the chemistry of buffers. The preparation of buffers, their effective range and how buffers resist changes in pH has been explained in understandable manner. The book also explains the preparation of commonly used lab reagents. Further, the chemistry of different lab test/functional group identification tests have been explained with mechanisms. Further, a comprehensive introduction about different types of titrimetry has been included. The chemistry of different acid-base indicators has been included along with mechanistic aspects. The authors envision that the readers of this book will find it worth reading to polish their concepts about the fundamentals of experiment chemistry. The authors have put a special emphasis on explaining different concepts with mechanistic approach. The authors will welcome the suggestions from readers enthusiastically.