Berezkin (petrochemical synthesis, USSR Academy of Sciences) explains to chromatographers that gas-liquid chromatography, an exciting development of gas chromatography, is itself just a limited case of gas-liquid-solid chromatography, and shows how this perspective can help solve problems more quick
Berezkin (petrochemical synthesis, USSR Academy of Sciences) explains to chromatographers that gas-liquid chromatography, an exciting development of gas chromatography, is itself just a limited case of gas-liquid-solid chromatography, and shows how this perspective can help solve problems more quick
A. V. Topchiev Institute of Petrochemical Synthesis Academy of Sciences of the USSR Moscow, USSR.
Inhaltsangabe
Preface Chapter 1 Introduction to Gas Liquid Solid Chromatography References Chapter 2 Absolute Retention of Analyzed Compounds 2.1 A model of the sorbent in gas liquid solid chromatography 2.2 Variation of the sorbent surface in gas liquid solid chromatography as a function of the content of the stationary liquid phase on the solid support 2.3 Principles of equilibrium theory of retention in gas liquid solid chromatography 2.4 Experimental verification of additive equilibrium theory References Chapter 3 Influence of Adsorption of Analyzed Compounds on Relative Retention Values and Invariant Relative Retention Values 3.1 Relative retention values in gas chromatography and chromatographic identification procedures 3.2 Effect of the solid support on relative retention values 3.3 Relative retention values in gas liquid solid chromatography and invariant relative retention values (theory and experimental determination) References Chapter 4 Effect of a Solid Support on the Efficiency of Chromatographic Separation 4.1 Effect of sorbent particle diameter 4.2 Role of a solid support porous structure 4.3 Effect of the adsorptional properties of a solid support References Chapter S Specific Features of Separation 5.1 Effect of the phase ratio (stationary liquid phase to solid adsorbent) on the characteristics of chromatographic resolution 5.2 Packed columns 5.2.1 Sorbent: stationary liquid phase on a solid support 5.2.2 Sorbent: stationary liquid phase on an active adsorbent 5.3 Capillary columns References Chapter 6 Effect of Adsorption and Catalytic Activity of a Solid Support on the Quantitative Analysis of Data 6.1 Irreversible or quasi irreversible adsorption of chromatographed compounds on the solid support and its effect on the results of quantitative analysis 6.2 Chemical transformation at the solid support surface References Chapter 7 Determination of Equilibrium Parameters of Absorption Interaction Between Chromatographed Substances and Stationary Liquid Phase References Chapter 8 Determination of Physicochemical Parameters for Adsorption of Chromatographed Compounds at the Gas Stationary Liquid Phase and Stationary Liquid Phase Solid Support Interfaces References Chapter 9 Effect of Solid Support on the Conditioning and Aging of Chromatographic Columns References Conclusion Index.
Preface Chapter 1 Introduction to Gas Liquid Solid Chromatography References Chapter 2 Absolute Retention of Analyzed Compounds 2.1 A model of the sorbent in gas liquid solid chromatography 2.2 Variation of the sorbent surface in gas liquid solid chromatography as a function of the content of the stationary liquid phase on the solid support 2.3 Principles of equilibrium theory of retention in gas liquid solid chromatography 2.4 Experimental verification of additive equilibrium theory References Chapter 3 Influence of Adsorption of Analyzed Compounds on Relative Retention Values and Invariant Relative Retention Values 3.1 Relative retention values in gas chromatography and chromatographic identification procedures 3.2 Effect of the solid support on relative retention values 3.3 Relative retention values in gas liquid solid chromatography and invariant relative retention values (theory and experimental determination) References Chapter 4 Effect of a Solid Support on the Efficiency of Chromatographic Separation 4.1 Effect of sorbent particle diameter 4.2 Role of a solid support porous structure 4.3 Effect of the adsorptional properties of a solid support References Chapter S Specific Features of Separation 5.1 Effect of the phase ratio (stationary liquid phase to solid adsorbent) on the characteristics of chromatographic resolution 5.2 Packed columns 5.2.1 Sorbent: stationary liquid phase on a solid support 5.2.2 Sorbent: stationary liquid phase on an active adsorbent 5.3 Capillary columns References Chapter 6 Effect of Adsorption and Catalytic Activity of a Solid Support on the Quantitative Analysis of Data 6.1 Irreversible or quasi irreversible adsorption of chromatographed compounds on the solid support and its effect on the results of quantitative analysis 6.2 Chemical transformation at the solid support surface References Chapter 7 Determination of Equilibrium Parameters of Absorption Interaction Between Chromatographed Substances and Stationary Liquid Phase References Chapter 8 Determination of Physicochemical Parameters for Adsorption of Chromatographed Compounds at the Gas Stationary Liquid Phase and Stationary Liquid Phase Solid Support Interfaces References Chapter 9 Effect of Solid Support on the Conditioning and Aging of Chromatographic Columns References Conclusion Index.
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