This Book focuses on Growth of Bi2Se3 Crystal and its characterizations. Growth of crystal by indigenously prepared Bridgman set up sets the tone of the book. Book Progress to discover Structural, Surface, Thermal and electrical properties of the grown crystal by X-ray Diffraction Analysis, Energy Dispersive Analysis of X-rays, UV-VIS absorption Spectroscopy, Transmission Electron Microscopy, Atomic Force Microscopy, Thermogravimatric analysis.Thermoelectric materials useful for thermoelectric cooling at room temperature and its potential application in superconductors and electronic apparatus characterization result and conclusions drawn in this book will help researchers working in the field of crystal growth and students pursuing their masters in solid state physics.