Rita Cornelis / Joe Caruso / Helen Crews / Klaus G. Heumann (Hgg.)

Handbook of Elemental Speciation

Techniques and Methodology
Herausgegeben:Cornelis, Rita; Caruso, Joseph A.; Crews, Helen; Heumann, Klaus G.

• Gebundenes Buch

Produktbeschreibung

This international collection of chapters comprehensively covers different aspects of procedures for speciation analysis at all levels starting from sample collection and storage, through sample preparation approaches to render the species chromatographable, principles of separation techniques used in speciation analysis, to the element specific detection.
_ International renowned editors and contributors
_ Includes coverage of electrochemical methods, biosensors for metal ions, radioisotope techniques and direct solid speciation techniques
_ Provides information on quality assurance and risk assessment, and speciation-relevant legislation

Each chapter is a stand-alone reference covering a given facet of elemental speciation analysis written by an expert in a given field with the volume as a whole providing an excellent introductory text and reference handbook.

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Produktdetails

• Verlag: Wiley & Sons
• 1. Auflage
• Seitenzahl: 672
• Erscheinungstermin: 8. August 2003
• Englisch
• Abmessung: 256mm x 193mm x 42mm
• Gewicht: 1585g
• ISBN-13: 9780471492146
• ISBN-10: 0471492140
• Artikelnr.: 11744887

Autorenporträt

Rita Cornelis, Department of Analytical Chemistry, Ghent University, The Netherlands.

Inhaltsangabe

List of Contributors.
Preface.
Technical Abbreviations and Acronyms.
1 Introduction.
2 Sampling: Collection, Storage.
2.1 Sampling: Collection, Processing and Storage of Environmental Samples.
2.2 Sampling of Clinical Samples: Collection and Storage.
2.3 Food: Sampling with Special Reference to Legislation, Uncertainty and
Fitness for Purpose.
2.4 Sampling: Collection, Storage - Occupational Health.
3 Sample Preparation.
3.1 Sample Treatment for Speciation Analysis in Biological Samples.
3.2 Sample Preparation Techniques for Elemental Speciation Studies.
3.3 Sample Preparation - Fractionation (Sediments, Soils, Aerosols and Fly
Ashes).
4 Separation Techniques.
4.1 Liquid Chromatography.
4.2 Gas Chromatography and Other Gas Based Methods.
4.3 Capillary Electrophoresis in Speciation Analysis.
4.4 Gel Electrophoresis for Speciation Purposes.
5 Detection.
5.1 Atomic Absorption and Atomic Emission Spectrometry.
5.2 Flow Injection Atomic Spectrometry for Speciation.
5.3 Detection by ICP-Mass Spectrometry.
5.4 Plasma Source Time-of-flight Mass Spectrometry: a Powerful Tool for
Elemental Speciation.
5.5 Glow Discharge Plasmas as Tunable Sources for Elemental Speciation.
5.6 Electrospray Methods for Elemental Speciation.
5.7 Elemental Speciation by Inductively Coupled Plasma-Mass Spectrometry
with High Resolution Instruments.
5.8 On-line Elemental Speciation with Functionalised Fused Silica
Capillaries in Combination with DIN-ICP-MS.
5.9 Speciation Analysis by Electrochemical Methods.
5.10 Future Instrumental Development for Speciation.
5.11 Biosensors for Monitoring of Metal Ions.
5.12 Possibilities Offered by Radiotracers for Method Development in
Elemental Speciation Analysis and for Metabolic and Environmentally Related
Speciation Studies.
6 Direct Speciation of Solids.
6.1 Characterization of Individual Aerosol Particles with Special Reference
to Speciation Techniques.
6.2 Direct Speciation of Solids: X-ray Absorption Fine Structure
Spectroscopy for Species Analysis in Solid Samples.
7 Calibration.
7.1 Calibration in Elemental Speciation Analysis.
7.2 Reference Materials.
8 Screening Methods for Semiquantitative Speciation Analysis.
9 Risk Assessments/Regulations.
9.1 Environmental Risk Assessment and the Bioavailability of Elemental
Species.
9.2 Speciation and Legislation.
Index.