Membrane reactors are increasingly replacing conventional separation, process and conversion technologies across a wide range of applications. Exploiting advanced membrane materials, they offer enhanced efficiency, are very adaptable and have great economic potential. There has therefore been increasing interest in membrane reactors from both the scientific and industrial communities, stimulating research and development. The two volumes of the Handbook of membrane reactors draw on this research to provide an authoritative review of this important field.Volume 1 explores fundamental materials…mehr
Membrane reactors are increasingly replacing conventional separation, process and conversion technologies across a wide range of applications. Exploiting advanced membrane materials, they offer enhanced efficiency, are very adaptable and have great economic potential. There has therefore been increasing interest in membrane reactors from both the scientific and industrial communities, stimulating research and development. The two volumes of the Handbook of membrane reactors draw on this research to provide an authoritative review of this important field.Volume 1 explores fundamental materials science, design and optimisation, beginning with a review of polymeric, dense metallic and composite membranes for membrane reactors in part one. Polymeric and nanocomposite membranes for membrane reactors, inorganic membrane reactors for hydrogen production, palladium-based composite membranes and alternatives to palladium-based membranes for hydrogen separation in membrane reactors are alldiscussed. Part two goes on to investigate zeolite, ceramic and carbon membranes and catalysts for membrane reactors in more depth. Finally, part three explores membrane reactor modelling, simulation and optimisation, including the use of mathematical modelling, computational fluid dynamics, artificial neural networks and non-equilibrium thermodynamics to analyse varied aspects of membrane reactor design and production enhancement.With its distinguished editor and international team of expert contributors, the two volumes of the Handbook of membrane reactors provide an authoritative guide for membrane reactor researchers and materials scientists, chemical and biochemical manufacturers, industrial separations and process engineers, and academics in this field.
Angelo Basile, a Chemical Engineer, is a senior Researcher at the ITM-CNR, University of Calabria, where he is responsible for research related to both the ultra-pure hydrogen production and CO2 capture using Pd-based Membrane Reactors. Angelo Basile's h-index is 53, with 387 document results with a total of 8,910 citations in 5,034 documents (www.scopus.com - 24 May 2023).
He has more than 170 scientific papers in peer-to-peer journals and 252 papers in international congresses; and is a reviewer for 165 int. journals, an editor/author of more than 50 scientific books and 120 chapters on international books on membrane science and technology; 6 Italian patents, 2 European patents and 5 worldwide patents. He is referee of 104 international scientific journals and Member of the Editorial Board of 22 of them.
Basile is also Editor associate of the Int. J. Hydrogen Energy and Editor-in-chief of the Int. J. Membrane Science & Technol. and Editor-in-chief of Membrane Processes (Applications), a section of the Intl J. Membranes. Basile also prepared 42 special issues on membrane science and technology for many international journals (IJHE, Chem Eng. J., Cat. Today, etc.). He participated to and was/is responsible of many national and international projects on membrane reactors and membrane science. Basile served as Director of the ITM-CNR during the period Dec. 2008 - May 2009. In the last years, he was tutor of 30 Thesis for master and Ph.D. students at the Chemical Engineering Department of the University of Calabria (Italy). From 2014, Basile is Full Professor of Chemical Engineering Processes.
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Woodhead Publishing Series in Energy
Foreword
Preface
Part I: Polymeric, dense metallic and composite membranes for membrane reactors
Chapter 1: Polymeric membranes for membrane reactors
Abstract:
1.1 Introduction: polymer properties for membrane reactors
1.2 Basics of polymer membranes
1.3 Membrane reactors
1.4 Modelling of polymeric catalytic membrane reactors
1.5 Conclusions
1.7 Appendix: nomenclature
Chapter 2: Inorganic membrane reactors for hydrogen production: an overview with particular emphasis on dense metallic membrane materials
Abstract:
2.1 Introduction
2.2 Development of inorganic membrane reactors (MRs)
2.3 Types of membranes
2.4 Preparation of dense metallic membranes
2.5 Preparation of Pd-composite membranes
2.6 Preparation of Pd-Ag alloy membranes
2.7 Preparation of Pd-Cu alloy composite membranes
2.8 Preparation of Pd-Au membranes
2.9 Preparation of amorphous alloy membranes
2.10 Degradation of dense metallic membranes
2.11 Conclusions and future trends
2.12 Acknowledgements
2.14 Appendix: nomenclature
Chapter 3: Palladium-based composite membranes for hydrogen separation in membrane reactors
Abstract:
3.1 Introduction
3.2 Development of composite membranes
3.3 Palladium and palladium-alloy composite membranes for hydrogen separation
3.4 Performances in membrane reactors
3.5 Conclusions and future trends
3.6 Acknowledgements
3.8 Appendix: nomenclature
Chapter 4: Alternatives to palladium in membranes for hydrogen separation: nickel, niobium and vanadium alloys, ceramic supports for metal alloys and porous glass membranes
Abstract:
4.1 Introduction
4.2 Materials
4.3 Membrane synthesis and characterization
4.4 Applications
4.5 Conclusions
4.7 Appendix: nomenclature
Chapter 5: Nanocomposite membranes for membrane reactors
Abstract:
5.1 Introduction
5.2 An overview of fabrication techniques
5.3 Examples of organic/inorganic nanocomposite membranes
5.4 Structure-property relationships in nanostructured composite membranes
5.5 Major application of hybrid nanocomposites in membrane reactors
5.6 Conclusions and future trends
5.8 Appendix: nomenclature
Part II: Zeolite, ceramic and carbon membranes and catalysts for membrane reactors
Chapter 6: Zeolite membrane reactors
Abstract:
6.1 Introduction
6.2 Separation using zeolite membranes
6.3 Zeolite membrane reactors
6.4 Modeling of zeolite membrane reactors
6.5 Scale-up and scale-down of zeolite membranes
6.6 Conclusion and future trends
6.8 Appendix: nomenclature
Chapter 7: Dense ceramic membranes for membrane reactors
Abstract:
7.1 Introduction
7.2 Principles of dense ceramic membrane reactors
7.3 Membrane preparation and catalyst incorporation
7.4 Fabrication of membrane reactors
7.5 Conclusion and future trends
7.6 Acknowledgements
7.8 Appendices
Chapter 8: Porous ceramic membranes for membrane reactors
Abstract:
8.1 Introduction
8.2 Preparation of porous ceramic membranes
8.3 Characterisation of ceramic membranes
8.4 Transport and separation of gases in ceramic membranes
8.5 Ceramic membrane reactors
8.6 Conclusions and future trends
8.7 Acknowledgements
8.9 Appendix: nomenclature
Chapter 9: Microporous silica membranes: fundamentals and applications in membrane reactors for hydrogen separation
Part I: Polymeric, dense metallic and composite membranes for membrane reactors
Chapter 1: Polymeric membranes for membrane reactors
Abstract:
1.1 Introduction: polymer properties for membrane reactors
1.2 Basics of polymer membranes
1.3 Membrane reactors
1.4 Modelling of polymeric catalytic membrane reactors
1.5 Conclusions
1.7 Appendix: nomenclature
Chapter 2: Inorganic membrane reactors for hydrogen production: an overview with particular emphasis on dense metallic membrane materials
Abstract:
2.1 Introduction
2.2 Development of inorganic membrane reactors (MRs)
2.3 Types of membranes
2.4 Preparation of dense metallic membranes
2.5 Preparation of Pd-composite membranes
2.6 Preparation of Pd-Ag alloy membranes
2.7 Preparation of Pd-Cu alloy composite membranes
2.8 Preparation of Pd-Au membranes
2.9 Preparation of amorphous alloy membranes
2.10 Degradation of dense metallic membranes
2.11 Conclusions and future trends
2.12 Acknowledgements
2.14 Appendix: nomenclature
Chapter 3: Palladium-based composite membranes for hydrogen separation in membrane reactors
Abstract:
3.1 Introduction
3.2 Development of composite membranes
3.3 Palladium and palladium-alloy composite membranes for hydrogen separation
3.4 Performances in membrane reactors
3.5 Conclusions and future trends
3.6 Acknowledgements
3.8 Appendix: nomenclature
Chapter 4: Alternatives to palladium in membranes for hydrogen separation: nickel, niobium and vanadium alloys, ceramic supports for metal alloys and porous glass membranes
Abstract:
4.1 Introduction
4.2 Materials
4.3 Membrane synthesis and characterization
4.4 Applications
4.5 Conclusions
4.7 Appendix: nomenclature
Chapter 5: Nanocomposite membranes for membrane reactors
Abstract:
5.1 Introduction
5.2 An overview of fabrication techniques
5.3 Examples of organic/inorganic nanocomposite membranes
5.4 Structure-property relationships in nanostructured composite membranes
5.5 Major application of hybrid nanocomposites in membrane reactors
5.6 Conclusions and future trends
5.8 Appendix: nomenclature
Part II: Zeolite, ceramic and carbon membranes and catalysts for membrane reactors
Chapter 6: Zeolite membrane reactors
Abstract:
6.1 Introduction
6.2 Separation using zeolite membranes
6.3 Zeolite membrane reactors
6.4 Modeling of zeolite membrane reactors
6.5 Scale-up and scale-down of zeolite membranes
6.6 Conclusion and future trends
6.8 Appendix: nomenclature
Chapter 7: Dense ceramic membranes for membrane reactors
Abstract:
7.1 Introduction
7.2 Principles of dense ceramic membrane reactors
7.3 Membrane preparation and catalyst incorporation
7.4 Fabrication of membrane reactors
7.5 Conclusion and future trends
7.6 Acknowledgements
7.8 Appendices
Chapter 8: Porous ceramic membranes for membrane reactors
Abstract:
8.1 Introduction
8.2 Preparation of porous ceramic membranes
8.3 Characterisation of ceramic membranes
8.4 Transport and separation of gases in ceramic membranes
8.5 Ceramic membrane reactors
8.6 Conclusions and future trends
8.7 Acknowledgements
8.9 Appendix: nomenclature
Chapter 9: Microporous silica membranes: fundamentals and applications in membrane reactors for hydrogen separation
Abstract:
9.1 Introduction
9.2 Microporous silica membranes
9.3 Membrane reactor function and arrangement
9.4 Membrane reactor performanc
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