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The motivation of Microwave Synthesis of Three Components Reactions and Aqueous Synthesis (water mediated) Reaction condition tools, synthesis under inert gas as new synthetic methodology of novel D-¿-A, D(2A), N-bridge Head Self-Assembly [ICT] Heterocyclic Moieties, Related Cyanine Dyes, (DD) 2-D-A, Ruthenium (ii) Complexes, Hole transport materials (HTM) in order to select the optimal conditions to be used as dye sensitized solar cells (DSSCs) is to improve the SpecificCharacterization, Photosensitization Behaviour & Probable Application in the field of Biology, Medical Science, Technology and Physics. N-Bridge Head Heterocyclic Functional & Related Islam M. Abdellah, Ph.D., 2018, Dyes were identified by elemental & Spectral Analyses. Special attention have been focus on the Absorption (Emission) Spectral, Solvato(Media)Chromic Behaviour (Acid-Base Properties), Photovoltaics, Electrochemical Impedance and Molecular Modeling (Theoretical Calculations) studies for some selected functional dyes.