Recently, organic inhibitors prepared synthetically are becoming popular in the field of corrosion control of metals, alloys and composite materials. As the methods of synthesis are possible in the chemistry lab of the institutions very easily and only in terms milligrams they are required for the studies. In this work three types of novel organic inhibitors are synthesized and characterized using glassware and instruments. They are successfully used to study the inhibition effect on corrosion properties like weight loss, potentiodynamic polarization and impedance studies of Aluminium 2024 alloy which is popular nowadays in aerospace, aeronautical, naval, automobile and industrial applications.