Marvin C. McMaster

LC/MS w/website

• Gebundenes Buch

Produktbeschreibung

LC/MS: A Practical User's Guide focuses on practical applications of LC/MS in compound identification and analysis of trace impurities. Like Dr. McMaster's previous books, it is designed as an easy-to-use reference for people working with LC/MS systems. The book discusses empirical methods for optimizing the method, maintaining the instrumentation, and using mass spectral library databases for compound identification. It includes a CD-ROM with PowerPoint slides and Frequently Asked Questions meant to facilitate the use of the book for learning and teaching purposes.

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A practical guide to using and maintaining an LC/MS system

The combination of liquid chromatography (LC) and mass spectrometry (MS) has become the laboratory tool of choice for a broad range of industries that require the separation, analysis, and purification of mixtures of organic compounds.

LC/MS: A Practical User's Guide provides LC/MS users with an easy-to-use, hands-on reference that focuses on the practical applications of LC/MS and introduces the equipment and techniques needed to use LC/MS successfully. Following a thorough explanation of the basic components and operation of the LC/MS system, the author presents empirical methods for optimizing the techniques, maintaining the instrumentation, and choosing the appropriate MS or LC/MS analyzer for any given problem.

LC/MS covers everything users need to know about:
_ The latest equipment, including quadrupole, time-of-flight, and ion trap analyzers
_ Cutting-edge processes, such as preparing HPLC mobile phases and samples; handling and maintaining a wide variety of silica, zirconium, and polymeric separation columns; interpreting and quantifying mass spectral data; and using MS interfaces
_ Current and future applications in the pharmaceutical and agrochemical industries, biotechnology, clinical research, environmental studies, and forensics

An accompanying PowerPoint(r) slide-set on CD-ROM provides vital teaching tools for instructors and new equipment operators. Abundantly illustrated and easily accessible, the text is designed to help students and practitioners acquire optimum proficiency in this powerful and rapidly advancing analytical application.

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Produktdetails

• Wiley-Interscience
• Verlag: Wiley & Sons
• Artikelnr. des Verlages: 14665531000
• 1. Auflage
• Seitenzahl: 184
• Erscheinungstermin: 1. August 2005
• Englisch
• Abmessung: 240mm x 161mm x 14mm
• Gewicht: 450g
• ISBN-13: 9780471655312
• ISBN-10: 0471655317
• Artikelnr.: 14857946

Autorenporträt

MARVIN C.MCMASTER, PHD, is a consultant and adjunct professor of chemistry at the University of Missouri?St. Louis, teaching courses on HPLC, GC/MS, and laboratory computing. He is a former researcher and product developer for DuPont, Kraft Foods, and Ciba-Geigy, and previously worked as a technical sales support specialist for instrument companies. Dr. McMaster is the author of HPLC: A Practical User's Guide and coauthor, with Christopher McMaster, of GC/MS: A Practical User's Guide (both from Wiley).

Inhaltsangabe

Chapter 1. Introduction to LC/MS.
Chapter 2. The HPLC System.
Chapter 3. The HPLC Column and Separation Modes.
Chapter 4. HPLC and Column Maintenance.
Chapter 5. Sample Preparation and Separations Development.
Chapter 6. LC/MS Interfaces.
Chapter 7. LC/MS Overview.
Chapter 8. The Mass Analyzers.
Chapter 9. Mass Spectrometer Maintence.
Chapter 10. Application Areas for LC/MS.
Chapter 11. Trace Analysis and LC/MS/MS.
Chapter 12. Drug Discovery and Benchtop LC/MS.
Chapter 13. Proteomics: LC/MALDI/TOF and MS/MS Libraries.
Chapter 14. The Future of LC/MS.
Appendix A: LC/MS Frequently Asked Questions.
Appendix B: Solvents and Volatile Buffers for LC/MS.
Appendix C: A Guide to Structure Interpretation.
Appendix D: A Glossary of LC/MS Terms.
Appendix E: LC/MS Selective Reading List.
 

Rezensionen

"In LC/MS: A Practical User s Guide, the author sets out to introduce LC/MS and provide some practical information for using it ... The present offering seeks to provide a practical resource for LC/MS in 150 pages ... The HPLC chapters will serve the beginning technician
Well." (J Am Soc Mass Spectrom, 2011)