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Diese Ausgabe wurde auf den neuesten Stand gebracht, um die, die mit der Anwendung oder dem Studium der Massenspektroskopie beginnen, zeitgemäß an das Thema heranzuführen. Der Autor deckt in den Kapiteln über Ionenquellen und Verfahren der Ionisierung, Massenanalyse, Ionennachweis und Fragmentierungsmuster die Grundlagen des Themas ab, schließt aber auch Kapitel über Tandem-Techniken (Gas- und Flüssigkeitschromatographie - Massenspektrometrie und Massenspektrometrie - Massenspektrometrie) und über atomare Massenspektrometrie einschließlich induktiv gekoppelter Plasma-Massenspektrometrie…mehr
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Diese Ausgabe wurde auf den neuesten Stand gebracht, um die, die mit der Anwendung oder dem Studium der Massenspektroskopie beginnen, zeitgemäß an das Thema heranzuführen. Der Autor deckt in den Kapiteln über Ionenquellen und Verfahren der Ionisierung, Massenanalyse, Ionennachweis und Fragmentierungsmuster die Grundlagen des Themas ab, schließt aber auch Kapitel über Tandem-Techniken (Gas- und Flüssigkeitschromatographie - Massenspektrometrie und Massenspektrometrie - Massenspektrometrie) und über atomare Massenspektrometrie einschließlich induktiv gekoppelter Plasma-Massenspektrometrie (ICPMS) ein. Wie bei allen Büchern der ACOL-Reihe sind Fragen zur Selbstüberprüfung und deren Lösungen enthalten.
Produktdetails
- Produktdetails
- Analytical Chemistry by Open Learning
- Verlag: Wiley & Sons
- 3. Aufl.
- Seitenzahl: 512
- Erscheinungstermin: 21. September 2007
- Englisch
- Abmessung: 244mm x 170mm x 28mm
- Gewicht: 846g
- ISBN-13: 9780470033111
- ISBN-10: 0470033118
- Artikelnr.: 22580229
- Analytical Chemistry by Open Learning
- Verlag: Wiley & Sons
- 3. Aufl.
- Seitenzahl: 512
- Erscheinungstermin: 21. September 2007
- Englisch
- Abmessung: 244mm x 170mm x 28mm
- Gewicht: 846g
- ISBN-13: 9780470033111
- ISBN-10: 0470033118
- Artikelnr.: 22580229
Edmond de Hoffmann, Université Catholique de Louvain, Belgium & Ludwig Institute for Cancer Research, Brussels, Belgium. Vincent Stroobant, Ludwig Institute for Cancer Research, Brussels, Belgium.
Contents Preface Introduction Principles Diagram of a Mass Spectrometer
History Ion Free Path 1 Ion Sources 1.1 Electron Ionization 1.2 Chemical
Ionization 1.3 Field Ionization 1.4 Fast Atom Bombardment and Liquid
Secondary Ion Mass Spectrometry 1.5 Field Desorption 1.6 Plasma Desorption
1.7 Laser Desorption 1.8 Matrix-Assisted Laser Desorption Ionization 1.9
Thermospray 1.10 Atmospheric Pressure Ionization 1.11 Electrospray 1.12
Atmospheric Pressure Chemical Ionization 1.13 Atmospheric Pressure
Photoionization (APPI) 1.14 Atmospheric Pressure Secondary Ion Mass
Spectrometry (APSIMS) 1.15 Inorganic Ionization Sources 1.16 Gas-Phase
Ion-Molecule Reactions 1.17 Formation and Fragmentation of Ions: Basic
Rules 2 Mass Analyzers 2.1 Quadrupole Analyzers 2.2 Ion Trap Analyzers 2.3
The Electrostatic Trap or "Orbitrap" 2.4 Time-of-Flight Analyzers 2.5
Magnetic and Electromagnetic Analyzers 2.6 Ion Cyclotron Resonance and
Fourier Transform Mass Spectrometry 2.7 Hybrid Instruments 3 Detectors and
Computers 3.1 Detectors 3.2 Computers 4 Tandem Mass Spectrometry (MS/MS)
4.1 Tandem Mass Spectrometry in Space or in Time 4.2 Tandem Mass
Spectrometry Scan Modes 4.3 Collision-activated or Collision-induced
Dissociation (CAD or CID) 4.4 Other Methods of Ion Activation 4.5 Reactions
Studied in MS/MS 4.6 Tandem Mass Spectrometry Applications 5 Mass
Spectrometry/Chromatography Coupling 5.1 Elution Chromatography Coupling
Techniques 5.2 Chromatography Data Acquisition Modes 5.3 Data Recording and
Treatment 6 Analytical Information 6.1 Mass Spectrometry Spectral
Collections 6.2 High Resolution 6.3 Isotopic Abundances 6.4 Low-mass
Fragments and Lost Neutrals 6.5 Number of Rings or Unsaturations 6.6 Mass
and Electron Parities, Closed-shell Ions and Open-shell Ions 6.7
Quantitative Data 7 Fragmentation Reactions 7.1 Electron Ionization and
Fragmentation Rates 7.2 Quasi-equilibrium and RRKM Theory 7.3 Ionization
and Appearance Energies 7.4 Fragmentation Reactions of Positive Ions 7.5
Fragmentation Reactions of Negative Ions 7.6 Charge Remote Fragmentation
(CRF) 7.7 Spectrum Interpretation 8 Analysis of Biomolecules 8.1
Biomolecules and Mass Spectrometry 8.2 Proteins and Peptides 8.3.
Oligonucleotides 8.4. Oligosaccharides 8.5. Lipids 8.6 Metabolomics 9
Exercises A. Questions B. Answers Appendices Appendix 1. Nomenclature 1.1.
Units 1.2. Definitions 1.3. Analyzers 1.4. Detection 1.5. Ionization 1.6
Ion Types 1.7. Ion-molecule Reaction 1.8. Fragmentation Appendix 2.
Abbreviations Appendix 3. Fundamental Physical Constants Appendix 4A .
Table of Isotopes in Ascending Mass Order Appendix 4B. Table of Isotopes in
Alphabetical Order Appendix 5. Isotopic Abundances in % for Various
Elemental Compositions CHON (M = 100%) Appendix 6. Gas-Phase Ion
Thermochemical Data of Molecules Appendix 7. Gas-Phase Ion Thermochemical
Data of Radicals Appendix 8. Literature on Mass Spectrometry Appendix 9.
Mass Spectrometry on Internet Index
History Ion Free Path 1 Ion Sources 1.1 Electron Ionization 1.2 Chemical
Ionization 1.3 Field Ionization 1.4 Fast Atom Bombardment and Liquid
Secondary Ion Mass Spectrometry 1.5 Field Desorption 1.6 Plasma Desorption
1.7 Laser Desorption 1.8 Matrix-Assisted Laser Desorption Ionization 1.9
Thermospray 1.10 Atmospheric Pressure Ionization 1.11 Electrospray 1.12
Atmospheric Pressure Chemical Ionization 1.13 Atmospheric Pressure
Photoionization (APPI) 1.14 Atmospheric Pressure Secondary Ion Mass
Spectrometry (APSIMS) 1.15 Inorganic Ionization Sources 1.16 Gas-Phase
Ion-Molecule Reactions 1.17 Formation and Fragmentation of Ions: Basic
Rules 2 Mass Analyzers 2.1 Quadrupole Analyzers 2.2 Ion Trap Analyzers 2.3
The Electrostatic Trap or "Orbitrap" 2.4 Time-of-Flight Analyzers 2.5
Magnetic and Electromagnetic Analyzers 2.6 Ion Cyclotron Resonance and
Fourier Transform Mass Spectrometry 2.7 Hybrid Instruments 3 Detectors and
Computers 3.1 Detectors 3.2 Computers 4 Tandem Mass Spectrometry (MS/MS)
4.1 Tandem Mass Spectrometry in Space or in Time 4.2 Tandem Mass
Spectrometry Scan Modes 4.3 Collision-activated or Collision-induced
Dissociation (CAD or CID) 4.4 Other Methods of Ion Activation 4.5 Reactions
Studied in MS/MS 4.6 Tandem Mass Spectrometry Applications 5 Mass
Spectrometry/Chromatography Coupling 5.1 Elution Chromatography Coupling
Techniques 5.2 Chromatography Data Acquisition Modes 5.3 Data Recording and
Treatment 6 Analytical Information 6.1 Mass Spectrometry Spectral
Collections 6.2 High Resolution 6.3 Isotopic Abundances 6.4 Low-mass
Fragments and Lost Neutrals 6.5 Number of Rings or Unsaturations 6.6 Mass
and Electron Parities, Closed-shell Ions and Open-shell Ions 6.7
Quantitative Data 7 Fragmentation Reactions 7.1 Electron Ionization and
Fragmentation Rates 7.2 Quasi-equilibrium and RRKM Theory 7.3 Ionization
and Appearance Energies 7.4 Fragmentation Reactions of Positive Ions 7.5
Fragmentation Reactions of Negative Ions 7.6 Charge Remote Fragmentation
(CRF) 7.7 Spectrum Interpretation 8 Analysis of Biomolecules 8.1
Biomolecules and Mass Spectrometry 8.2 Proteins and Peptides 8.3.
Oligonucleotides 8.4. Oligosaccharides 8.5. Lipids 8.6 Metabolomics 9
Exercises A. Questions B. Answers Appendices Appendix 1. Nomenclature 1.1.
Units 1.2. Definitions 1.3. Analyzers 1.4. Detection 1.5. Ionization 1.6
Ion Types 1.7. Ion-molecule Reaction 1.8. Fragmentation Appendix 2.
Abbreviations Appendix 3. Fundamental Physical Constants Appendix 4A .
Table of Isotopes in Ascending Mass Order Appendix 4B. Table of Isotopes in
Alphabetical Order Appendix 5. Isotopic Abundances in % for Various
Elemental Compositions CHON (M = 100%) Appendix 6. Gas-Phase Ion
Thermochemical Data of Molecules Appendix 7. Gas-Phase Ion Thermochemical
Data of Radicals Appendix 8. Literature on Mass Spectrometry Appendix 9.
Mass Spectrometry on Internet Index
Contents Preface Introduction Principles Diagram of a Mass Spectrometer
History Ion Free Path 1 Ion Sources 1.1 Electron Ionization 1.2 Chemical
Ionization 1.3 Field Ionization 1.4 Fast Atom Bombardment and Liquid
Secondary Ion Mass Spectrometry 1.5 Field Desorption 1.6 Plasma Desorption
1.7 Laser Desorption 1.8 Matrix-Assisted Laser Desorption Ionization 1.9
Thermospray 1.10 Atmospheric Pressure Ionization 1.11 Electrospray 1.12
Atmospheric Pressure Chemical Ionization 1.13 Atmospheric Pressure
Photoionization (APPI) 1.14 Atmospheric Pressure Secondary Ion Mass
Spectrometry (APSIMS) 1.15 Inorganic Ionization Sources 1.16 Gas-Phase
Ion-Molecule Reactions 1.17 Formation and Fragmentation of Ions: Basic
Rules 2 Mass Analyzers 2.1 Quadrupole Analyzers 2.2 Ion Trap Analyzers 2.3
The Electrostatic Trap or "Orbitrap" 2.4 Time-of-Flight Analyzers 2.5
Magnetic and Electromagnetic Analyzers 2.6 Ion Cyclotron Resonance and
Fourier Transform Mass Spectrometry 2.7 Hybrid Instruments 3 Detectors and
Computers 3.1 Detectors 3.2 Computers 4 Tandem Mass Spectrometry (MS/MS)
4.1 Tandem Mass Spectrometry in Space or in Time 4.2 Tandem Mass
Spectrometry Scan Modes 4.3 Collision-activated or Collision-induced
Dissociation (CAD or CID) 4.4 Other Methods of Ion Activation 4.5 Reactions
Studied in MS/MS 4.6 Tandem Mass Spectrometry Applications 5 Mass
Spectrometry/Chromatography Coupling 5.1 Elution Chromatography Coupling
Techniques 5.2 Chromatography Data Acquisition Modes 5.3 Data Recording and
Treatment 6 Analytical Information 6.1 Mass Spectrometry Spectral
Collections 6.2 High Resolution 6.3 Isotopic Abundances 6.4 Low-mass
Fragments and Lost Neutrals 6.5 Number of Rings or Unsaturations 6.6 Mass
and Electron Parities, Closed-shell Ions and Open-shell Ions 6.7
Quantitative Data 7 Fragmentation Reactions 7.1 Electron Ionization and
Fragmentation Rates 7.2 Quasi-equilibrium and RRKM Theory 7.3 Ionization
and Appearance Energies 7.4 Fragmentation Reactions of Positive Ions 7.5
Fragmentation Reactions of Negative Ions 7.6 Charge Remote Fragmentation
(CRF) 7.7 Spectrum Interpretation 8 Analysis of Biomolecules 8.1
Biomolecules and Mass Spectrometry 8.2 Proteins and Peptides 8.3.
Oligonucleotides 8.4. Oligosaccharides 8.5. Lipids 8.6 Metabolomics 9
Exercises A. Questions B. Answers Appendices Appendix 1. Nomenclature 1.1.
Units 1.2. Definitions 1.3. Analyzers 1.4. Detection 1.5. Ionization 1.6
Ion Types 1.7. Ion-molecule Reaction 1.8. Fragmentation Appendix 2.
Abbreviations Appendix 3. Fundamental Physical Constants Appendix 4A .
Table of Isotopes in Ascending Mass Order Appendix 4B. Table of Isotopes in
Alphabetical Order Appendix 5. Isotopic Abundances in % for Various
Elemental Compositions CHON (M = 100%) Appendix 6. Gas-Phase Ion
Thermochemical Data of Molecules Appendix 7. Gas-Phase Ion Thermochemical
Data of Radicals Appendix 8. Literature on Mass Spectrometry Appendix 9.
Mass Spectrometry on Internet Index
History Ion Free Path 1 Ion Sources 1.1 Electron Ionization 1.2 Chemical
Ionization 1.3 Field Ionization 1.4 Fast Atom Bombardment and Liquid
Secondary Ion Mass Spectrometry 1.5 Field Desorption 1.6 Plasma Desorption
1.7 Laser Desorption 1.8 Matrix-Assisted Laser Desorption Ionization 1.9
Thermospray 1.10 Atmospheric Pressure Ionization 1.11 Electrospray 1.12
Atmospheric Pressure Chemical Ionization 1.13 Atmospheric Pressure
Photoionization (APPI) 1.14 Atmospheric Pressure Secondary Ion Mass
Spectrometry (APSIMS) 1.15 Inorganic Ionization Sources 1.16 Gas-Phase
Ion-Molecule Reactions 1.17 Formation and Fragmentation of Ions: Basic
Rules 2 Mass Analyzers 2.1 Quadrupole Analyzers 2.2 Ion Trap Analyzers 2.3
The Electrostatic Trap or "Orbitrap" 2.4 Time-of-Flight Analyzers 2.5
Magnetic and Electromagnetic Analyzers 2.6 Ion Cyclotron Resonance and
Fourier Transform Mass Spectrometry 2.7 Hybrid Instruments 3 Detectors and
Computers 3.1 Detectors 3.2 Computers 4 Tandem Mass Spectrometry (MS/MS)
4.1 Tandem Mass Spectrometry in Space or in Time 4.2 Tandem Mass
Spectrometry Scan Modes 4.3 Collision-activated or Collision-induced
Dissociation (CAD or CID) 4.4 Other Methods of Ion Activation 4.5 Reactions
Studied in MS/MS 4.6 Tandem Mass Spectrometry Applications 5 Mass
Spectrometry/Chromatography Coupling 5.1 Elution Chromatography Coupling
Techniques 5.2 Chromatography Data Acquisition Modes 5.3 Data Recording and
Treatment 6 Analytical Information 6.1 Mass Spectrometry Spectral
Collections 6.2 High Resolution 6.3 Isotopic Abundances 6.4 Low-mass
Fragments and Lost Neutrals 6.5 Number of Rings or Unsaturations 6.6 Mass
and Electron Parities, Closed-shell Ions and Open-shell Ions 6.7
Quantitative Data 7 Fragmentation Reactions 7.1 Electron Ionization and
Fragmentation Rates 7.2 Quasi-equilibrium and RRKM Theory 7.3 Ionization
and Appearance Energies 7.4 Fragmentation Reactions of Positive Ions 7.5
Fragmentation Reactions of Negative Ions 7.6 Charge Remote Fragmentation
(CRF) 7.7 Spectrum Interpretation 8 Analysis of Biomolecules 8.1
Biomolecules and Mass Spectrometry 8.2 Proteins and Peptides 8.3.
Oligonucleotides 8.4. Oligosaccharides 8.5. Lipids 8.6 Metabolomics 9
Exercises A. Questions B. Answers Appendices Appendix 1. Nomenclature 1.1.
Units 1.2. Definitions 1.3. Analyzers 1.4. Detection 1.5. Ionization 1.6
Ion Types 1.7. Ion-molecule Reaction 1.8. Fragmentation Appendix 2.
Abbreviations Appendix 3. Fundamental Physical Constants Appendix 4A .
Table of Isotopes in Ascending Mass Order Appendix 4B. Table of Isotopes in
Alphabetical Order Appendix 5. Isotopic Abundances in % for Various
Elemental Compositions CHON (M = 100%) Appendix 6. Gas-Phase Ion
Thermochemical Data of Molecules Appendix 7. Gas-Phase Ion Thermochemical
Data of Radicals Appendix 8. Literature on Mass Spectrometry Appendix 9.
Mass Spectrometry on Internet Index