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This monograph describes the results of scientific research conducted by the authors in 2017-2020 on the radioecological assessment of environmental objects of the Surkhandarya region. Areas of the region may pose a risk from natural and man-made radiation. Analysis of the results of determining the amount of natural radionuclides cesium-137, strontium-90, radon-222, and potassium-40 isotopes in atmospheric air, natural waters, and soil bioresources by radiometric-spectrometric method. doneThe monograph is intended for use by independent researchers, primary doctoral students, research interns, master's and bachelor's students, and professionals working in this field in training courses.