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The high temperature decontamination of reactor coolant is a crucial process in heavy water reactors. Nuclear power plants rely on heavy water reactors to generate electricity. Heavy water is used as a coolant to absorb the heat generated by the nuclear reactions in the reactor core. Over time, the coolant can become contaminated with radioactive materials, which can lead to corrosion of the reactor components and pose risks to the environment and human health. Optimizing the high temperature decontamination process is vital for the effective maintenance of heavy water reactors. Chemical processes are used to remove contaminants from the coolant and prevent further contamination. The process must be carefully designed to ensure maximum efficiency and minimum impact on the environment. Author has focuses on optimizing the high temperature decontamination process for reactor coolant. His work involves developing and testing new chemical cleaning agents, designing efficient decontamination protocols, and evaluating the environmental impact of the process. Also book explains, one of the key challenges in the high temperature decontamination process is maintaining the safety and reliability of the reactor during the decontamination procedure. The process must be carefully planned and executed to minimize the risk of accidents and damage to the reactor. Author also explains the impact of the decontamination process on the material properties of the reactor components. Thermal stress and corrosion can occur during the process, which can reduce the lifespan of the components and affect the performance of the reactor. This book contributes to the ongoing efforts to improve the efficiency and effectiveness of this critical process. Overall, optimizing the high temperature decontamination process is crucial for ensuring the safety and reliability of heavy water reactors.