Organic Syntheses, Volume 91

Herausgeber: Brummond, Kay M

• Gebundenes Buch

Produktbeschreibung

The demand for synthetic procedures that can be duplicated may be less egregious today than in 1921, but there is still a need. To date, Organic Syntheses has filled this need with 90 volumes of "checked" experimentals; and with the culmination of Kay Brummond's term as a member of the editorial board, the addition of Volume 91.

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Produktdetails

• Verlag: Wiley
• Volume 91 edition
• Seitenzahl: 416
• Erscheinungstermin: 26. Mai 2015
• Englisch
• Abmessung: 231mm x 155mm x 25mm
• Gewicht: 680g
• ISBN-13: 9781119054160
• ISBN-10: 1119054168
• Artikelnr.: 42517318

Autorenporträt

Kay M. Brummond, Ph.D., is a researcher in the field synthetic organic chemistry. She has published 50 journal articles, 15 reviews and book chapters and delivered over 140 invited lectures and symposia. The students and postdoctoral fellows in her group have presented 52 conference posters and presentations. Nineteen graduate students have obtained Ph.D. and M.S. degrees under her direction. She is a recipient of the Chancellor's Distinguished Research Award from the University of Pittsburgh, the 2006 ACS Akron Section Award, the Carnegie Science Center Emerging Female Scientist Award and the Johnson & Johnson Focused Giving Award. She is on the Board of Editors of > and Library Synthesis where she is also a project leader.

Inhaltsangabe

Discussion Addendum: Resolution of 1,1'-Bi-2-Naphthol; (R)-(+)- and (S)-(-)-2,2'-Bis(diphenylphosphino)-1,1'-binaphthyl(BINAP) 1 David L. Hughes Discussion Addendum for: Practical Synthesis of Novel Chiral Allenamides: (R)-4-Phenyl-3-(1,2-propadienyl)oxazoldin-2-one 12 Yong-Chua Teo and Richard P. Hsung N-Carboxylated-2-substituted Indoles and 2,3-Disubstituted-2,3-dihydro-4-quinolones from 2-Alkynylbenzamides 27 Noriko Okamoto, Kei Takeda, and Reiko Yanada Pd-Catalyzed External-CO-Free Carbonylation: Preparation of 2,4,6-Trichlorophenyl 3,4-Dihydronaphthalene-2-Carboxylate 39 Hideyuki Konishi, Tsuyoshi Ueda, and Kei Manabe Rhodium-Catalyzed Direct Amination of Arene C-H Bonds Using Azides as the Nitrogen Source 52 Sae Hume Park, Yoosu Park, and Sukbok Chang Synthesis of Alkynyliodonium Salts: Preparation of Phenyl (phenylethynyl)iodonium Trifluoroacetate 60 Luke I. Dixon, Michael A. Carroll, George J. Ellames and Thomas J. Gregson Palladium-catalyzed 1,4-Addition of Terminal Alkynes to Conjugated Enones 72 Feng Zhou, Liang Chen and Chao-Jun Li Cross-Coupling of Alkenyl/Aryl Carboxylates with Grignard Reagents via Fe-Catalyzed C-O Bond Activation 83 Bi-Jie Li, Xi-Sha Zhang and Zhang-Jie Shi Preparation of 5-Hydroxycyclopentenones Via Conjugate Addition-Initiated Nazarov Cyclization 93 Joshua L. Brooks, Yu-Wen Huang, and Alison J. Frontier Synthesis of Arylboronic Pinacol Esters from Corresponding Arylamines 106 Di Qiu, He Meng, Liang Jin, Shengbo Tang, Shuai Wang, Fangyang Mo, Yan Zhang and Jianbo Wang Preparation of Alkanesulfonyl Chlorides from S-Alkyl Isotghiourea Salts via N-Chlorosuccinimide Mediated Oxidative Chlorosulfonation 116 Zhanhui Yang and Jiaxi Xu DABCO-bis(sulfur dioxide), DABSO, as an easy-to-handle source of SO2: Sulfonamide preparation 125 Edward J. Emmett and Michael C. Willis One-pot Preparation of (S)-N-[(S)-1-Hydroxy-4-metghyl-1,1-diphenylpentan-2-yl]pyrrolidine-2-carboxamide from L-Proline 137 Wacharee Hamying, Nonognaphat Duangdee, and Albrecht Berkessel Enantioselective Rhodium-Catalyzed [2+2+2] Cycloaddition of Pentenyl Isocyanate and 4-Ethynylanisole: Preparation and Use of Taddol-pyrrolidine Phosphoramidite 150 Kevin M. Oberg, Timothy J. Martin, Mark Emil Oinen, Derek M. Dalton, Rebecca Keller Friedman, Jamie M. Neely, and Tomislav Rovis Synthesis and Use of a Trifluoromethylated Azomethine Ylide Precursor: Ethyl 1-Benzyl-trans-5-(trifluoromethyl)pyrrolidine-3-carboxylate 162 Daniel M. Allwood, Duncan L. Browne and Steven V. Ley Enantioselective Organocatalytic-
-Arylation of Aldehydes 175 Pernille H. Poulsen, Mette Overgaard, Kim L. Jensen and Kari Anker Jørgensen Synthesis of 4,5-Disubstituted 2-aminothiazoles from
,ß-Unsaturated Ketones: Preparation of S-benzyl-4-methyl-2-aminothiazolium Hydrochloride salt 185 Antonio Bermejo Gómez, Nanna Ahlsten, Ana E. Platero-Prats and Belen Martin-Matute Sodium Methoxide-Catalyzed Direct Amidation of Esters 201 Kazushi Agura, Takashi Ohshima, Yukiko Hayashi, And Kazushi Mashima Synthesis of Tetrasubstituted 1H-Pyrazoles by Copper-mediated Coupling of Enaminones with Nitriles 211 Mamta Suri and Frank Glorius Synthesis of 1,3-Dimethyl-3-(p-tolyl)-1H-pyrrolo[3,2-c]pyridin-2(3H)-one by Cu(II)-Mediated Direct Oxidative Coupling 221 Chandan Dey and E. Peter Kundig Preparation of (R)-4-Cyclohexyl-2,3-butadien-1-ol 233 Juntao Ye and Shengming Discussion Addendum for: Formation of y-Keto Esters from ß-Keto Esters: Methyl 5,5-dimethyl-4-oxohexanoate 248 Yashoda M. D. Bhogadhi and Charles K. Zercher Ni-catalyzed Reductive Cleavage of Methyl 3-Methoxy-2-Naphthoate 260 Josep Cornella, Cayetana Zarate, and Ruben Martin Indium-Catalyzed Heteroaryl-Heteroaryl Bond Formation through Nucleophilic Aromatic Substitution: Preparation of 2-Methyl-3-(thien-2-yl)-1H-indole 273 Yuta Nagase and Teruhisa Tsuchimoto Synthesis of 2,3-Disubstituted Benzofurans by the Palladium-Catalyzed Coupling of 2-Iodoanisoles and Terminal Alkynes, Followed by Electrophilic Cyclization: 3-Iodo-2-phenylbenzofuran 283 Tuanli Yao, Dawei Yue, and Richard C. Larock Enantioselective Preparation of (S)-5-Oxo-5,6-dihydro-2H-oyran-2-yl Benzoate 293 Tamas Benkovics, Adrian Ortiz, Zhiwei Guo, Animesh Goswami and Prashant Deshpande Iron-Catalyzed Selective Conjugate Addition of Aryl Grignard Reagents to 2,4-Alkadienoates: tert-Butyl (Z)-5-Phenyl-3-hexenoate 307 Takeshi Hata, Hideyuki Goto, Tomofumi Yokomizo, and Hirokazu Urabe 3-Hydrixymethyl-3-phenylcyclopropene 322 Ramajeyam Selvaraj, Srinvasa R. Chintala, Michael T. Taylor and Joseph M. Fox Enantioselective Synthesis of
- and ß-Boc-protected 6-Hydroxy-pyranones: Carbohydrate Building Blocks 338 Sumit O. Bajaj, Jamison R. Farnsworth and George A. O'Doherty