The current volume continues the tradition of the Organic Syntheses series, providing carefully checked and edited experimental procedures that describe important synthetic methods, transformations, reagents, and synthetic building blocks or intermediates with demonstrated utility in organic synthesis. These significant and interesting procedures should prove worthwhile to many synthetic chemists working in increasingly diverse areas. A trusted guide for professionals in organic and medicinal chemistry in academia, government, and industries, including pharmaceuticals, fine chemicals, agrochemicals, and biotechnological products.…mehr
The current volume continues the tradition of the Organic Syntheses series, providing carefully checked and edited experimental procedures that describe important synthetic methods, transformations, reagents, and synthetic building blocks or intermediates with demonstrated utility in organic synthesis. These significant and interesting procedures should prove worthwhile to many synthetic chemists working in increasingly diverse areas. A trusted guide for professionals in organic and medicinal chemistry in academia, government, and industries, including pharmaceuticals, fine chemicals, agrochemicals, and biotechnological products.Hinweis: Dieser Artikel kann nur an eine deutsche Lieferadresse ausgeliefert werden.
Late-Stage Deoxyfluorination of Phenols with PhenoFluorMix 16 Junting Chen and Tobias Ritter
Nickel-Catalyzed Cross-Coupling of 2-Methoxynaphthalene with Methyl 4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)benzoate 36 Yuki Kawashima, Takayuki Furukawa, Naoto Chatani and Mamoru Tobisu
Discussion Addendum for: Lithium Amides as Homochiral Ammonia Equivalents for Conjugate Additions to alpha,ß-Unsaturated Esters: Asymmetric Synthesis of (S)-ß-Leucine 53 Stephen G. Davies, Ai M. Fletcher, Paul M. Roberts, and James E. Thomson
Synthesis of 2,3-Diaryl-2H-azirines via Cs2CO3-Mediated Cyclization of Ketoxime Acetates 66 Mi-Na Zhao and Zheng-Hui Guan
Discussion Addendum for: The Direct Acyl-Alkylation of Arynes. Preparation of Methyl 2- (2-acetylphenyl)acetate 80 Austin C. Wright and Brian M. Stoltz
Discussion Addendum for: Convenient Preparation of 3-Ethoxycarbonyl Benzofurans from Salicylaldehydes and Ethyl Diazoacetate 98 Mizzanoor Rahaman and M. Mahmun Hossain
Discussion Addendum for: Phosphine-Catalyzed [4 + 2] Annulation: Synthesis of Ethyl 6-Phenyl-1-tosyl-1,2,5,6-tetrahydropyridine-3-carboxylate 110 Aslam C. Shaikh and Ohyun Kwon
Discussion Addendum for: Protection of Alcohols using 2-Benzyloxy-1-methylpyridinium Trifluoromethanesulfonate: Methyl (R)-(-)-3-Benzyloxy-2-methyl Propanoate 124 Harvey F. Fulo, Philip A. Albiniak, and Gregory B. Dudley
Synthesis of 4-Methylbenzoate(2',4',6'-trimethoxy-phenyl)iodonium Tosylate 137 Thomas L. Seidl, Aaron Moment, Charles Orella, Thomas Vickery, and David R. Stuart
Gold-Catalyzed Oxidative Coupling of Arenes and Arylsilanes 150 Chris Nottingham, Verity Barber, and Guy C. Lloyd-Jones
Discussion Addendum for: Preparation of Enantioenriched Homoallylic Primary Amines 179 Miguel Yus
Discussion Addendum for: Synthesis of Ynamides by Copper-Mediated Coupling of 1,1-Dibromo-1-alkenes with Nitrogen Nucleophiles. Preparation of 4-Methyl-N-(2-phenylethynyl)-N-(phenylmethyl)benzenesulfonamide 195 Cédric Theunissen, Pierre Thilmany, Mounsef Lahboubi, Nicolas Blanchard, and Gwilherm Evano
Discussion Addendum for: Phosphine-Catalyzed [3 + 2] Annulation: Synthesis of Ethyl 5-(tert-Butyl)-2-phenyl-1-tosyl-3-pyrroline-3-carboxylate 214 Aslam C. Shaikh and Ohuyn Kwon
Discussion Addendum for: Synthesis of Highly Enantiomerically Enriched Amines by Asymmetric Transfer Hydrogenation of N-(tert-Butylsulfinyl) Imines 232 Miguel Yus
Synthesis of Chiral Diamine Ligands for Nickel-catalyzed Asymmetric Cross-couplings of Alkylchloroboronate Esters with Alkylzincs: 1R,2R)-N,N'-Dimethyl-1,2-bis(2-methylphenyl)-1,2-diaminoethane 245 Yusuke Masuda and Gregory C. Fu
Preparation of 5-(Triisopropylalkynyl) dibenzo[b,d] thiophenium triflate 258 Bernd Waldecker, Kevin Kafuta, and Manuel Alcarazo
Three-Step Synthesis of 2-(Diiodomethyl)-4,4,5,5-tetramethyl- 1,3,2-dioxaborolane from Dichloromethane 277 Morgane Sayes, Guillaume Benoit, and André B. Charette
Discussion Addendum for: Allylic Oxidation Catalyzed by Dirhodium(II) Tetrakis[epsilon-caprolactamate] of tert-Butyldimethylsilylprotected trans-Dehydroandrosterone 300 Yong-Liang Su, Luca De Angelis and Michael P. Doyle
Preparation of (R)-3-(3,5-Bistrifluoromethylphenyl)-1,1'-bi-2-naphthol 312 Yusuke Kobayashi, Atsushi Matsuda, Tomoya Ushimaru, and Toshiro Harada
Catalytic Enantioselective Addition of an In-Situ Prepared Aryltitanium Reagent to p-Chloroacetophenone: (R)-(+)-1-(4-Chlorophenyl)-1-m-tolylethanol 333 Yusuke Kobayashi, Atsushi Matsuda, Tomoya Ushimaru, and Toshiro Harada
Stereoselective Synthesis of (R)-((R)-1-Phenyl-2,2,2-trichloroethyl)-2-(2-bromophenyl)aziridine-1-carboxy
Late-Stage Deoxyfluorination of Phenols with PhenoFluorMix 16 Junting Chen and Tobias Ritter
Nickel-Catalyzed Cross-Coupling of 2-Methoxynaphthalene with Methyl 4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)benzoate 36 Yuki Kawashima, Takayuki Furukawa, Naoto Chatani and Mamoru Tobisu
Discussion Addendum for: Lithium Amides as Homochiral Ammonia Equivalents for Conjugate Additions to alpha,ß-Unsaturated Esters: Asymmetric Synthesis of (S)-ß-Leucine 53 Stephen G. Davies, Ai M. Fletcher, Paul M. Roberts, and James E. Thomson
Synthesis of 2,3-Diaryl-2H-azirines via Cs2CO3-Mediated Cyclization of Ketoxime Acetates 66 Mi-Na Zhao and Zheng-Hui Guan
Discussion Addendum for: The Direct Acyl-Alkylation of Arynes. Preparation of Methyl 2- (2-acetylphenyl)acetate 80 Austin C. Wright and Brian M. Stoltz
Discussion Addendum for: Convenient Preparation of 3-Ethoxycarbonyl Benzofurans from Salicylaldehydes and Ethyl Diazoacetate 98 Mizzanoor Rahaman and M. Mahmun Hossain
Discussion Addendum for: Phosphine-Catalyzed [4 + 2] Annulation: Synthesis of Ethyl 6-Phenyl-1-tosyl-1,2,5,6-tetrahydropyridine-3-carboxylate 110 Aslam C. Shaikh and Ohyun Kwon
Discussion Addendum for: Protection of Alcohols using 2-Benzyloxy-1-methylpyridinium Trifluoromethanesulfonate: Methyl (R)-(-)-3-Benzyloxy-2-methyl Propanoate 124 Harvey F. Fulo, Philip A. Albiniak, and Gregory B. Dudley
Synthesis of 4-Methylbenzoate(2',4',6'-trimethoxy-phenyl)iodonium Tosylate 137 Thomas L. Seidl, Aaron Moment, Charles Orella, Thomas Vickery, and David R. Stuart
Gold-Catalyzed Oxidative Coupling of Arenes and Arylsilanes 150 Chris Nottingham, Verity Barber, and Guy C. Lloyd-Jones
Discussion Addendum for: Preparation of Enantioenriched Homoallylic Primary Amines 179 Miguel Yus
Discussion Addendum for: Synthesis of Ynamides by Copper-Mediated Coupling of 1,1-Dibromo-1-alkenes with Nitrogen Nucleophiles. Preparation of 4-Methyl-N-(2-phenylethynyl)-N-(phenylmethyl)benzenesulfonamide 195 Cédric Theunissen, Pierre Thilmany, Mounsef Lahboubi, Nicolas Blanchard, and Gwilherm Evano
Discussion Addendum for: Phosphine-Catalyzed [3 + 2] Annulation: Synthesis of Ethyl 5-(tert-Butyl)-2-phenyl-1-tosyl-3-pyrroline-3-carboxylate 214 Aslam C. Shaikh and Ohuyn Kwon
Discussion Addendum for: Synthesis of Highly Enantiomerically Enriched Amines by Asymmetric Transfer Hydrogenation of N-(tert-Butylsulfinyl) Imines 232 Miguel Yus
Synthesis of Chiral Diamine Ligands for Nickel-catalyzed Asymmetric Cross-couplings of Alkylchloroboronate Esters with Alkylzincs: 1R,2R)-N,N'-Dimethyl-1,2-bis(2-methylphenyl)-1,2-diaminoethane 245 Yusuke Masuda and Gregory C. Fu
Preparation of 5-(Triisopropylalkynyl) dibenzo[b,d] thiophenium triflate 258 Bernd Waldecker, Kevin Kafuta, and Manuel Alcarazo
Three-Step Synthesis of 2-(Diiodomethyl)-4,4,5,5-tetramethyl- 1,3,2-dioxaborolane from Dichloromethane 277 Morgane Sayes, Guillaume Benoit, and André B. Charette
Discussion Addendum for: Allylic Oxidation Catalyzed by Dirhodium(II) Tetrakis[epsilon-caprolactamate] of tert-Butyldimethylsilylprotected trans-Dehydroandrosterone 300 Yong-Liang Su, Luca De Angelis and Michael P. Doyle
Preparation of (R)-3-(3,5-Bistrifluoromethylphenyl)-1,1'-bi-2-naphthol 312 Yusuke Kobayashi, Atsushi Matsuda, Tomoya Ushimaru, and Toshiro Harada
Catalytic Enantioselective Addition of an In-Situ Prepared Aryltitanium Reagent to p-Chloroacetophenone: (R)-(+)-1-(4-Chlorophenyl)-1-m-tolylethanol 333 Yusuke Kobayashi, Atsushi Matsuda, Tomoya Ushimaru, and Toshiro Harada
Stereoselective Synthesis of (R)-((R)-1-Phenyl-2,2,2-trichloroethyl)-2-(2-bromophenyl)aziridine-1-carboxy
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