Product innovation in the food sector, as well as concern about food quality in general, is growing and is regulated worldwide. As a result, there is a greater demand for increasingly qualified professionals to carry out activities in the bromatological field, including, in addition to composition control, physical-chemical and microbiological quality control for the purposes of developing new products; processing control and even inspections for possible findings of fraud. This book presents a collection of experimental protocols carried out at the Faculdade de Integração do Sertão-FIS, the aim of which was to give undergraduates experience of the techniques most commonly used in food analysis.