Powder Diffraction

Theory and Practice
Herausgeber: Dinnebier, R E; Billinge, S J L

• Gebundenes Buch

Produktbeschreibung

Powder diffraction is a widely used scientific technique in the characterization of materials with broad application in materials science, chemistry, physics, geology, pharmacology and archaeology. Powder Diffraction Theory and Practice provides an advanced introductory text about modern methods and applications of powder diffraction in research and industry. The authors begin with a brief overview of the basic theory of diffraction from crystals and powders. Data collection strategies are described including x-ray, neutron and electron diffraction setups using modern day apparatus including synchrotron sources. Data corrections, essential for quantitative analysis are covered before the authors conclude with a discussion of the analysis methods themselves. The information is presented in a way that facilitates understanding the information content of the data, as well as best practices for collecting and analyzing data for quantitative analysis. This long awaited book condenses the knowledge of renowned experts in the field into a single, authoritative, overview of the application of powder diffraction in modern materials research. The book contains essential theory and introductory material for students and researchers wishing to learn how to apply the frontier methods of powder diffraction.

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Produktdetails

• Verlag: RSC Publishing
• Seitenzahl: 604
• Erscheinungstermin: 10. März 2008
• Englisch
• Abmessung: 233mm x 164mm x 38mm
• Gewicht: 1066g
• ISBN-13: 9780854042319
• ISBN-10: 0854042318
• Artikelnr.: 23806624

Inhaltsangabe

Chapter 1: Principles of Powder Diffraction
Chapter 2: Experimental Setups
Chapter 3: The Intensity of a Bragg Reflection
Chapter 4: General Data Reduction
Chapter 5: The Profile of a Bragg Reflection for Extracting Intensities
Chapter 6: Instrumental Contributions to the Line Profile in X-ray Powder Diffraction. Example of the Diffractometer with Bragg-Brentano Geometry
Chapter 7: Indexing and Space Group Determination
Chapter 8: Crystal Structure Determination
Chapter 9: Rietveld Refinement
Chapter 10: The Derivative Difference Minimization Method
Chapter 11: Quantitative Phase Analysis
Chapter 12: Microstructural Properties: Texture and Macrostress Effects
Chapter 13: Microstructural Properties: Lattice Defects and Domain Size Effects
Chapter 14: Two-dimensional Powder Diffraction using Area Detectors: The Experimental Setup
Chapter 15: Powder Diffraction at Non-ambient Conditions
Chapter 16: Local Structure from Total Scattering and Atomic Pair Distribution Function (PDF) Analysis
Chapter 17: Computer Software for Powder Diffraction