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This text book describe the experimental procedure of drugs and organic compounds like synthesis of Phenytoin, Benzocaine, Sulphacetamide, Barbutric Acid Anthranilic Acid, Benzophenone Oxime. It contains Analysis of drugs and organic compounds Diclofenac Sodium Gel, Caffeine, Lignocaine, Phenytoin. Detail Procedure for the Qualitative Analysis of Carbohydrate, Protein and Lipids. Quantitative Analytical Procedure of Biochemical Components.