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The purpose of this textbook is to present about the Manufacturing processof Tri Ethyl ortho Acetate and the preliminary steps before conducting into large scale industries. An idea of material and Energy balance .The book provides various approaching methods when handling and making a product of particular component.Triethyl orthoacetate can be used for the synthesis of: Ordered mesoporous carbons for catalysis, electrochemistry and hydrogen storage applications. Esters of phosphonic acids, carboxylic acids and phosphinic acids.