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This book provides basically the primary information regarding toxic metallic pollution scenario of Guwahati City, the gateway of North East India.The pronounced contamination is observed for Al, Pb, Zn, Cr, Cd and Cu in the road side surface soil and road runoff water of Guwahati City.The data provided in the book may be helpful to carry out further investigation of the state of metal in the road side surface soil and road runoff water.Data of metal may be considered for metal related diseases and effects on the biotic and a biotic components in and around the study area.