The text book discussed the modern laboratory synthesis of hybrid peptides and peptide mimetic, showing the importance and scope of the materials. The book is a modern account of design and synthetic methods and an up-to-date description of recent advances in hybrid peptides and peptide mimetic and their diverse application. The book will be of significant interest to chemistry, biotechnology, spectroscopy and material science students at undergraduate and graduate level. The book will be helpful for researchers in academia and industry who are working with polymers, foldamers, hybrid peptides and peptide mimetic.