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Detailed and step by step variation of the Structural properties of as synthesized nanoparticles and physics associated with it is explained. Size of as synthesized nanoparticles plays important role in altering the properties of Optical, thermal, magnetic, Electrical & Dielectric properties of the material is also discussed in depth in this book. Further X ray diffraction, EDAX and Transmission / Scanning electron microscopy is presented for every synthesized samples.