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Benzazoles the most relevant bioactive heterocyclic compounds comprising oxygen, nitrogen and sulfur atoms. They are used as precious molecules acting as antimicrobial, antiin fi ammatory, Antitubercular, anti HIV, anticonvulsant and anticancer agents. This book consists introduction of benzazoles, they devided into three chapters, chapter 1: Preparation and biological applications of benzothiazole, chapter 2: Preparation and biological applications of benzoxazole and Chapter 3: Preparation and biological applications of benzimidazole. Many synthetic chemistry and medicinal chemistry researchers around the world working on these Benzazoles, pyrazole and this book gives lot of useful information to the fresh researchers as well as the most senior researchers.