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This book is based on the removal of heavy metal ions by the use of different adsorbents. The resultant resin was prepared through method suspension polymerization method. Synthesis and Characterization of Macroporous AN- Dimethacrylate Copolymer Beads. Extraction of lead ions from aquatic system by using diethylenetriamine modified polyacrylonitrile-ethylene glycoldimetacrylate. Preparation of ethyleneamine functionalized crosslinked poly(acrylonitrile-ethylene glycoldimethacrylate) chelating resins for adsorption of lead ions. Studies on Uptake Behavior of Hg(II) and Pb(II) by Amine modified glycidyl methacrylate-styrene-N,N'-methylenebisacrylamide terpolymer. A convenient one step preparation of crosslinked polystyrene mercaptomethyl resin. Applications of mercaptomethyl crosslinked polystyrene resin for extraction of mercury and arsenic ions from wastewater.