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A study of Synthesis, Characterization and Biological investigation of Schiff base is an attempt to fulfill the pressing demand of graduate and postgraduate students of colleges as well as universities for chemistry research on the basis of scientific knowledge. It is worthwhile to suggest one more experiments along with its characterization and biological data and its results and discussion to determine the Synthesis, Characterization and Biological study of Schiff bases of the organic compounds. The present work was aimed at synthesis of new Schiff bases of some Active pharmaceutical ingredients with different types of aldehydes and their study of pharmaceutical properties and characteristics. Author has tried to write this book in a lucid and systematic manner. I hope this work will be helpful to the young researchers.