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Vanadium (III) complexes with eight different O-Donor ligands were synthesized. Characterizational Elucidation of the Synthesized Complexes is done by UV-Visible Spectroscopy, IR Spectroscopy & Mass Spectrometry. Thermal pyrolysis of the complexes & its kinetics is studied by Thermo-gravimetric Analysis. Estimation of Vanadium in the complexes is carried out by ICP-AES. Biological Activities of the complexes (2)-(5), (7) & (8) have also been tested against various bacteria & fungi.