The physical chemistry practical book covers the necessary basic information need to do well in laboratory. Detailed information on instrumentation, experimental methods and solution preparations provide a foundation to undergraduate and postgraduate students for understanding the basic principles and its importance in routine chemical analysis. Looking at the need of students, an attempt has been made to present the physical practical covering in a simple and understandable manner. I hope that students find this book useful and expected to have all relevant background material in these sources prior to coming to the laboratory.