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This book provides an overview of the synthesis processes, including physicochemical and green approaches, as well as numerous characterization methods and applications of nanotechnology in a wide range of domains. The book has five chapters: The first chapter discusses the history of nanotechnology, current trends in nanotechnology, behaviors, and different types of nanomaterials. The second chapter describes the various nanoparticle synthesis processes. This chapter describes the various physicochemical synthesis processes with appropriate diagrams. The third chapter addresses the environmentally friendly processes used in nanoparticle synthesis. The fourth chapter discusses characterization processes that are critical in assessing nanoparticle quality. The fifth chapter discusses the use of NPs in numerous fields, including science and technology. It addresses the potential health risks posed by many regularly used nanoparticles.