Applications of Solid Phase Microextraction (eBook, PDF)

Redaktion: Pawliszyn, Janusz

• Format: PDF

Produktbeschreibung

Solid Phase Microextraction (SPME) has been introduced as a modern alternative to current sample preparation technology, and has a wide range of applications. Focusing on quantitative aspects of analysis, Applications of Solid Phase Microextraction aims to describe these applications.

In industry, practical uses of SPME can be found in environmental, food, pharmaceutical, clinical and forensic applications, all of which are described in this book. Important scientific applications such as reaction monitoring, characterization of coatings and distributions of analytes in natural multiphase systems are also discussed. Throughout there are descriptions of new technologies, including new coatings and interfaces for analytical instrumentation (SPME/LC and SPME/CE), automation and calibration processes.

Written by internationally recognised experts, edited by the scientist involved in the research since its infancy, and encompassing a wide range of applications, this book will be ideal for anyone wishing to explore the feasibility of using SPME technology.

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Produktdetails

• Verlag: RSC
• Seitenzahl: 674
• Erscheinungstermin: 31. Oktober 2007
• Englisch
• ISBN-13: 9781847550149
• Artikelnr.: 44761962

Inhaltsangabe

Foreword
Contents
Contributors
Glossary
Calibration and quantitation by SPME
Quantitative aspects of SPME
Quantitation by SPME before reaching a partition equilibrium
Coatings and interfaces
SPME coupled to capillary electrophoresis
Selectivity in SPME
Properties of commericial SPME coatings
Sol-gel technology for thermally stable coatings in SPME
Solid versusliquids coatings
Physiochemical applications
Application of SPME to study sorption phenomena on dissolved humic organic matter
The use of SPME to measure free concentrations and phospholipid/water and protein/water partition coefficients
Estimation of hydrophobicity of organic compounds
Environmental applications
Air sampling with SPME
The application of sPME in water analysis
The application of SPME to pestivide residue analysis
Inter-laboratory validation of SPME for the quantitative analysis of aqueous samples
SPME for the determination of organochlorine pestivides in natural waters
Determination of sulfur-containing compounds in wastewater
Analysis of creosote and oil in aqueous contaminations by SPME
Direct analysis of solids using sPME
Analysis of solid samples by hot water extraction -SPME
Field analysis by SPME
Organometallic speciation by combining aqueous phase derivatization with SPME-GC-FPD-MS
Metal speciation by SPME-CGC-ICPMS
The application of SPME-LC-MS to the determination of contaminants in complex environmental matrices
SPME-HPLC of environmental pollutants
Analysis of industrial pollutants in environmental samples
Food, flavour, fragrance and pheromone applications
Analysis of food and plant volatiles
Application of SPME to measure volatile metabolites produced by staphylococcus carnosus and staphylococcus xylosus
Application of SPME methods for the determination of volatile wine aroma compounds in view of the varietal characterization
Analysis of vodkas and white rums by SPMS-GC-MS
Analysis of food volatiles using SPME
Analysis of volatile contaminants in foods
Determination of pesticides in foods by automated SPMS-GC-MS
SPME in the study of chemical communication in social wasps
Pharmaceutical, clinical and forensic applications
Propyl chloroformate derivatisation and SPME-GC for screening Of amines in urine
Isolation of drugs and poisons in biological fluids by SPME
On-fiber derivatization for analysis of steroids by SPME and GC-MS
SPME-Quadrupole ion trap mass spectrometry for the determination of drugs of abuse in biological matrices
Analysis of drugs in biological fluids using SPME
SPME-Microcolumm LC: Application to toxicological drug analysis
Optimization of drug analysis by SPME
Applications of SPME for the biomonitoring of human exposure to toxic substances
Applications of SPME in criminal investigations
Reaction monitoring
SPME-GC-MS detection analysis of maillard reaction products
SPME investigation of intermediates produced during biodegradation of contaminated materials
Related techniques
Infrared spectroscopic detection for SPME
SPME in Near-IR Fiber-optic Evanescent Field Absorption Spectroscopy: A Method for Rapid, Remote In situ Monitoring of Nonpolar Organic Compounds in Water
Author Index