Michael K. Miller, Richard G. Forbes

Atom-Probe Tomography (eBook, PDF)

The Local Electrode Atom Probe

• Format: PDF

Produktbeschreibung

This book aims to provide an introduction and overview of atom-probe tomography from a materials science perspective, a full introduction to underlying theory and to current understanding of the theory of laser-pulsed APT, and a careful account of how to prepare specimens, set up the appropriate conditions for tomography, analyse the experimental data, and present results.

A special feature of this book is that it includes an updated historical account of the development of the underlying theory (including field evaporation), allowing readers to appreciate how theoretical understanding of the science behind the technique reached its present state.

This book is ideal for:

· beginners as well as more experienced researchers and scientists

· those interested mainly in using the pulsed-laser local electrode atom probe for materials science

· those interested in developing the technique and understanding the details of how it works

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Produktdetails

• Verlag: Springer New York
• Seitenzahl: 423
• Erscheinungstermin: 31. Juli 2014
• Englisch
• ISBN-13: 9781489974303
• Artikelnr.: 43795824

Inhaltsangabe

Introduction: Atom Probe Tomography.- Historical Development.- Underlying Physics.- Applications to Microstructural Characterization. Instrumentation: Local Electrode Atom Probe.- Voltage and Laser Pulsing Methods.- Nano-Positioning Stage.- Energy Compensation.- Field Ion microscopy.- Specimen Preparation.- Requirements.- Electropolishing.- FIB-Based Methods.- Specimen Failure Mechanisms.- Data Reconstruction: Raw Data Conversion.- Element Assignment of Micro/Nano, Mass Spectra, Molecular and Complex Ions.- Resolutions.- Preferential Evaporation and Retention.- Detection Efficiency.- Atom Maps.- Simulations.- Analysis of Data: Composition Determination, Standard Error, Smoothing Methods.- Local Order Methods.- Concentration Profiles.- Contingency Tables.- Binomial Distributions.- Friend-of-Friends and Nearest Neighbor Methods- Appendices.