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This book offers a thorough theoretical description of the method, an overview on the current status of the various forms of electrokinetic capillary chromatography, plus a look forward into future developments. * Focuses on the technique of electrokinetic capillary chromatography and its applications in various areas, including pharmaceutical, industrial, environmental, and biological chemistry * Features invaluable information put together from experienced researchers in the area * First book to discuss this technique in detail * Covers a topic that is part of the exploding field of…mehr
This book offers a thorough theoretical description of the method, an overview on the current status of the various forms of electrokinetic capillary chromatography, plus a look forward into future developments. * Focuses on the technique of electrokinetic capillary chromatography and its applications in various areas, including pharmaceutical, industrial, environmental, and biological chemistry * Features invaluable information put together from experienced researchers in the area * First book to discuss this technique in detail * Covers a topic that is part of the exploding field of hyphenated techniques * Selected international contributors working in research in this area
Dieser Download kann aus rechtlichen Gründen nur mit Rechnungsadresse in A, B, BG, CY, CZ, D, DK, EW, E, FIN, F, GR, HR, H, IRL, I, LT, L, LR, M, NL, PL, P, R, S, SLO, SK ausgeliefert werden.
Dr Ute Pyell received his PhD in Analytical Chemistry in 1991. He is an active member in the of the German Chemical Society (GDCh), the of the Analytical Division of the GDCh and an active member in the Working Group Education and Training of the .
Inhaltsangabe
List of Contributors vii Preface xi Part I: Separation Principles 1 1 Theory of Electrokinetic Chromatography 3 Ute Pyell 2 Determination of Critical Micelle Concentrations by Capillary Electrokinetic Techniques 33 Thomas Le Saux, Anne Varenne and Pierre Gareil 3 Selectivity Characterization of Pseudostationary Phases Using the Solvation Parameter Model 55 Colin F. Poole 4 General Aspects of Resolution Optimization with Micellar Pseudostationary Phases 79 li Jia and Shigeru Terabe 5 Optimization of the Separation Conditions in Electrokinetic Chromatography: Experimental Designs, Modelling and Validation 95 Olga Jiménez and Maria Luisa Marina 6 Microemulsion Electrokinetic Chromatography 115 Alex Marsh, Kevin Altria and Brian Clark 7 Polymeric Pseudostationary Phases and Dendrimers 137 Christopher P. Palmer 8 Pseudostationary Ion-exchange Phases 153 Philip J. Zakaria and Paul R. Haddad 9 Principles of Enantiomer Separations in Electrokinetic Chromatography 179 Bezhan Chankvetadze 10 On-line Sample Enrichment in Electrokinetic Chromatography 207 Joselito P. Quirino Part II: Instrumentation 233 11 General Aspects of Instrumentation 235 Jan Fischer and Pavel Jandera 12 Laser-induced Fluorescence Detection: A Summary 263 Christophe Bayle, Véréna Poinsot, Clara Fournier-Noël and François Couderc 13 Amperometric Detection 281 Frank-Michael Matysik 14 Photothermal Detection 289 Werner Faubel, Stefan Heissler and Ute Pyell 15 Coupling of Electrokinetic Chromatography to Mass Spectrometry 307 Roelof Mol, Gerhardus J. de Jong and Govert W. Somsen 16 Electrokinetic Chromatography on Microfluidic Devices 337 Ómar Gústafsson and Jörg P. Kutter Part III: Applications 351 17 Electromigration Separation Techniques in Pharmaceutical Analysis 353 Jean-Luc Veuthey, Laurent Geiser and Serge Rudaz 18 Analysis of Body Fluids by Electrokinetic Chromatographic Techniques 373 Ll. Puignou, R. Busquets and M.T. Galceran 19 Application of Electrokinetic Chromatography to Food and Beverages 423 Mary Boyce 20 Application of Enantioselective Electrokinetic Chromatography 459 Bezhan Chankvetadze 21 Environmental Analysis 475 Ana Carolina O. Costa, Gustavo A. Micke, Elisabete A. Pereira, Clóvis L. Silva and Marina F.M. Tavares Index 529
List of Contributors vii Preface xi Part I: Separation Principles 1 1 Theory of Electrokinetic Chromatography 3 Ute Pyell 2 Determination of Critical Micelle Concentrations by Capillary Electrokinetic Techniques 33 Thomas Le Saux, Anne Varenne and Pierre Gareil 3 Selectivity Characterization of Pseudostationary Phases Using the Solvation Parameter Model 55 Colin F. Poole 4 General Aspects of Resolution Optimization with Micellar Pseudostationary Phases 79 li Jia and Shigeru Terabe 5 Optimization of the Separation Conditions in Electrokinetic Chromatography: Experimental Designs, Modelling and Validation 95 Olga Jiménez and Maria Luisa Marina 6 Microemulsion Electrokinetic Chromatography 115 Alex Marsh, Kevin Altria and Brian Clark 7 Polymeric Pseudostationary Phases and Dendrimers 137 Christopher P. Palmer 8 Pseudostationary Ion-exchange Phases 153 Philip J. Zakaria and Paul R. Haddad 9 Principles of Enantiomer Separations in Electrokinetic Chromatography 179 Bezhan Chankvetadze 10 On-line Sample Enrichment in Electrokinetic Chromatography 207 Joselito P. Quirino Part II: Instrumentation 233 11 General Aspects of Instrumentation 235 Jan Fischer and Pavel Jandera 12 Laser-induced Fluorescence Detection: A Summary 263 Christophe Bayle, Véréna Poinsot, Clara Fournier-Noël and François Couderc 13 Amperometric Detection 281 Frank-Michael Matysik 14 Photothermal Detection 289 Werner Faubel, Stefan Heissler and Ute Pyell 15 Coupling of Electrokinetic Chromatography to Mass Spectrometry 307 Roelof Mol, Gerhardus J. de Jong and Govert W. Somsen 16 Electrokinetic Chromatography on Microfluidic Devices 337 Ómar Gústafsson and Jörg P. Kutter Part III: Applications 351 17 Electromigration Separation Techniques in Pharmaceutical Analysis 353 Jean-Luc Veuthey, Laurent Geiser and Serge Rudaz 18 Analysis of Body Fluids by Electrokinetic Chromatographic Techniques 373 Ll. Puignou, R. Busquets and M.T. Galceran 19 Application of Electrokinetic Chromatography to Food and Beverages 423 Mary Boyce 20 Application of Enantioselective Electrokinetic Chromatography 459 Bezhan Chankvetadze 21 Environmental Analysis 475 Ana Carolina O. Costa, Gustavo A. Micke, Elisabete A. Pereira, Clóvis L. Silva and Marina F.M. Tavares Index 529
Rezensionen
"...an excellent reference for those chemists who follow developments in the area of small molecule separations or...separations in EKC." ( Journal of the American Chemical Society , January 31, 2007)
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