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Plants and plant-derived compounds and drugs are becoming more and more popular with increasing numbers of scientists researching plant analysis. The quality control of herbal drugs is also becoming essential to avoid severe health problems, and in the future many more new drugs will be developed from plant sources. This three-volume Handbook, featuring 47 detailed review articles, is unique as it deals with chemical and biological methodologies for plant analysis. It presents the most important and most accurate methods which are available for plant analysis. This comprehensive work is…mehr
Plants and plant-derived compounds and drugs are becoming more and more popular with increasing numbers of scientists researching plant analysis. The quality control of herbal drugs is also becoming essential to avoid severe health problems, and in the future many more new drugs will be developed from plant sources. This three-volume Handbook, featuring 47 detailed review articles, is unique as it deals with chemical and biological methodologies for plant analysis. It presents the most important and most accurate methods which are available for plant analysis. This comprehensive work is divided into six sections as follows: Sample preparation and identification - discussing plant selection and collection, followed by extraction and sample preparation methodologies. Extraction and sample preparation methodologies Instrumentation for chemical analysis - several instrumentations for chemical plant analysis are presented with an emphasis on hyphenated techniques, e.g. the coupling between HPLC and mass spectroscometry, and HPLC with NMR. Strategies for selective classes of compounds - coverage of the most interesting classes of compounds such as polysaccharides, saponins, cardiotonic glycosides, alkaloids, terpenoids, lipids, volatile compounds and polyphenols ( flavonoids, xanthones, coumarins, naphthoquinones, anthraquinones, proanthocyanidins, etc.). Biological Analysis - includes phenotyping, DNA barcoding techniques, transcriptome analysis , microarray, metabolomics and proteomics. Drugs from Plants - covers the screening of plant extracts and strategies for the quick discovery of novel bioactive natural products. Safety assessment of herbal drugs is highly dependent on outstanding chromatographic and spectroscopic methods which are also featured here. This Handbook introduces to scientists involved in plant studies the current knowledge of methodologies in various fields of chemically- and biochemically-related topics in plant research. The content from this Handbook will publish online within the Encyclopedia of Analytical Chemistry via Wiley Online Library: href="http://www.wileyonlinelibrary.com/ref/eac">http://www.wileyonlinelibrary.com/ref/eac Benefit from the introductory offer, valid until 30 November 2014! Introductory price: £425.00 / $695.00 / EUR550.00 List price thereafter: £495.00 / $795.00 / EUR640.00
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Autorenporträt
Kurt Hostettmann is the editor of Handbook of Chemical and Biological Plant Analytical Methods, 3 Volume Set, published by Wiley. Shilin Chen is the editor of Handbook of Chemical and Biological Plant Analytical Methods, 3 Volume Set, published by Wiley. Andrew Marston is the editor of Handbook of Chemical and Biological Plant Analytical Methods, 3 Volume Set, published by Wiley. Hermann Stuppner is the editor of Handbook of Chemical and Biological Plant Analytical Methods, 3 Volume Set, published by Wiley.
Inhaltsangabe
VOLUME I List of Contributors xi Preface xvii In Memoriam Andrew Marston xix Part One: Sample Preparation and Identification 1 1 Selection, Identification, and Collection of Plants 3 Monique S. J. Simmonds 2 Extraction Methodologies: General Introduction 17 Valerie Camel 3 Supercritical Fluid Extraction 43 Seied Mahdi Pourmortazavi, Mehdi Rahimi-Nasrabadi and Somayeh Mirsadeghi 4 New Trends in Extraction of Natural Products: Microwave-Assisted Extraction and Pressurized Liquid Extraction 77 Philippe Christen and Beatrice Kaufmann 5 Solid-Phase Microextraction (SPME) and Its Application to Natural Products 105 M. Abdul Mottaleb, Mohammed J. Meziani and M. Rafiq Islam Part Two: Instrumentation for Chemical Analysis 129 6 Microscopic Analysis 131 Johannes Saukel and Elisabeth Ginko 7 Thin-Layer Chromatography, with Chemical and Biological Detection Methods 185 Aurelie Urbain and Claudia Avello Simoes-Pires 8 HPLC and Ultra HPLC: Basic Concepts 207 Veronika R. Meyer 9 Near-Infrared (NIR) Spectroscopy in Natural Product Research 227 Christian W. Huck 10 Headspace Sampling and Gas Chromatography: A Successful Combination to Study the Composition of a Plant Volatile Fraction 245 Barbara Sgorbini, Cecilia Cagliero, Chiara Cordero, Erica Liberto, Patrizia Rubiolo and Carlo Bicchi 11 Analysis of Natural Products by Capillary Electrophoresis and Related Techniques 277 Markus Ganzera and Anja Kruger 12 LC and LC-MS: Techniques and Applications 307 Nadja Arens, Stefanie Doell and Hans-Peter Mock 13 NMR as Analytical Tool for Crude Plant Extracts 317 Anna R. Bilia 14 NMR of Small Molecules 349 Christoph Seger 15 NMR of Large Molecules 361 Christoph H. Wunderlich, Sarina Grutsch, Martin Tollinger and Christoph Kreutz 16 On-Line and At-Line LC-NMR and Related Micro-NMR Methods 379 Nadine Bohni, Emerson F. Queiroz and Jean-Luc Wolfender 17 New Developments of Laser Desorption Ionization Mass Spectrometry in Plant Analysis 411 Andreas Schinkovitz, Denis Seraphin and Pascal Richomme VOLUME II List of Contributors xi Preface xvii In Memoriam Andrew Marston xix Part Three: Strategies for Selective Classes of Compounds 425 18 Analysis of Plant Oligo- and Polysaccharides 427 Wolfgang Blaschek 19 Analytical Strategies for Multipurpose Studies of a Plant Volatile Fraction 447 Cecilia Cagliero, Barbara Sgorbini, Chiara Cordero, Erica Liberto, Carlo Bicchi and Patrizia Rubiolo 20 Strategies for Lipid Analysis 467 Irina A. Guschina and John L. Harwood 21 HPLC Analysis of Alkaloids 485 Bras Heleno de Oliveira 22 Identification and Characterization of Hydroxycinnamates of Six Galium Species from the Rubiaceae Family 505 Rakesh Jaiswal, Marius F. Matei, Sagar Deshpande and Nikolai Kuhnert 23 Identification and Characterization of Trimeric Proanthocyanidins of Two Members of the Rhododendron Genus (Ericaceae) by Liquid Chromatography Multi-Stage Mass Spectrometry 525 Rakesh Jaiswal, Mohamed G. E. Karar and Nikolai Kuhnert 24 Strategies in the Analysis of Flavonoids 543 Celestino Santos-Buelga and Ana M. Gonzalez-Paramas 25 Coumarins - Analytical and Preparative Techniques 569 Krystyna Skalicka-Wözniak and Kazimierz G¿owniak 26 Naphthoquinones and Anthraquinones: Chemical, Analytical, and Biological Overview 595 Nahed El-Najjar, Hala Gali-Muhtasib, Pia Vuorela, Arto Urtti and Heikki Vuorela 27 Xanthones from Marine-Derived Microorganisms: Isolation, Structure Elucidation, and Biological Activities 611 Madalena M. M. Pinto, Raquel A. P. Castanheiro and Anake Kijjoa 28 Sesquiterpenes and Other Terpenoids 633 Eirini Kouloura, Job Tchoumtchoua, Maria Halabalaki and Alexios-Leandros Skaltsounis 29 Analysis of Plant Saponins 687 Justyna Krzyzanowska, Mariusz Kowalczyk and Wieslaw Oleszek 30 Cardiotonic Glycosides 709 Liselotte Krenn 31 Plant Steroids: Occurrence, Biological Significance, and Their Analysis 727 G. M. Kamal B. Gunaherath and A. A. Leslie Gunatilaka 32 Chemical Analysis of Bryophytes 753 Yoshinori Asakawa, Agnieszka Ludwiczuk and Masao Toyota 33 Cyclotide Analysis 807 Susan E. Northfield, Aaron G. Poth, Charlotte D'Souza and David J. Craik VOLUME III List of Contributors xi Preface xvii In Memoriam Andrew Marston xix Part Four: Biological Analysis 825 34 Phenotyping 827 Qiaosheng Guo and Zaibiao Zhu 35 Identification of Medicinal Plants Using DNA Barcoding 843 Xiaohui Pang and Shilin Chen 36 Transcriptome Analysis of Medicinal Plants with Next-Generation Sequencing Technologies 847 Shilin Chen and Hongmei Luo 37 Microarray 859 Chang Liu, Haimei Chen, Jianqin Li and Xiaolan Xu 38 Small RNAs 875 Shanfa Lu 39 Metabolomics 885 Jan Schripsema and Denise Dagnino 40 Proteomics and Its Research Techniques in Plants 903 Liming Yang, Haibin Xu and Shilin Chen 41 Multivariate Data Analysis 915 Bieke Dejaegher Part Five: Drugs from Plants 947 42 In Silico-Guided Strategies for the Discovery and Rationalization of Bioactive Natural Products 949 Petra H. Pfisterer, Daniela Schuster, Judith M. Rollinger and Hermann Stuppner 43 Innovative Strategies in the Search for Bioactive Plant Constituents 967 Emerson F. Queiroz and Jean-Luc Wolfender 44 High Throughput Screening of Vegetal Natural Substances 987 Bruno David and Frederic Ausseil 45 Mycotoxins Contamination in Food: Alternative Plant Preservatives, Legislation, and Detection Methods 1011 Monica R. Zuzarte, Ana P. Martins, Maria J. Goncalves and Lígia R. Salgueiro 46 Quality Assessment of Herbal Drugs and Medicinal Plant Products 1039 Iqbal Ahmad, Mohd Sajjad Ahmad Khan and Swaranjit Singh Cameotra Part Six: Conclusion and Perspectives 1057 47 Conclusion and Perspectives 1059 Index 1061
VOLUME I List of Contributors xi Preface xvii In Memoriam Andrew Marston xix Part One: Sample Preparation and Identification 1 1 Selection, Identification, and Collection of Plants 3 Monique S. J. Simmonds 2 Extraction Methodologies: General Introduction 17 Valerie Camel 3 Supercritical Fluid Extraction 43 Seied Mahdi Pourmortazavi, Mehdi Rahimi-Nasrabadi and Somayeh Mirsadeghi 4 New Trends in Extraction of Natural Products: Microwave-Assisted Extraction and Pressurized Liquid Extraction 77 Philippe Christen and Beatrice Kaufmann 5 Solid-Phase Microextraction (SPME) and Its Application to Natural Products 105 M. Abdul Mottaleb, Mohammed J. Meziani and M. Rafiq Islam Part Two: Instrumentation for Chemical Analysis 129 6 Microscopic Analysis 131 Johannes Saukel and Elisabeth Ginko 7 Thin-Layer Chromatography, with Chemical and Biological Detection Methods 185 Aurelie Urbain and Claudia Avello Simoes-Pires 8 HPLC and Ultra HPLC: Basic Concepts 207 Veronika R. Meyer 9 Near-Infrared (NIR) Spectroscopy in Natural Product Research 227 Christian W. Huck 10 Headspace Sampling and Gas Chromatography: A Successful Combination to Study the Composition of a Plant Volatile Fraction 245 Barbara Sgorbini, Cecilia Cagliero, Chiara Cordero, Erica Liberto, Patrizia Rubiolo and Carlo Bicchi 11 Analysis of Natural Products by Capillary Electrophoresis and Related Techniques 277 Markus Ganzera and Anja Kruger 12 LC and LC-MS: Techniques and Applications 307 Nadja Arens, Stefanie Doell and Hans-Peter Mock 13 NMR as Analytical Tool for Crude Plant Extracts 317 Anna R. Bilia 14 NMR of Small Molecules 349 Christoph Seger 15 NMR of Large Molecules 361 Christoph H. Wunderlich, Sarina Grutsch, Martin Tollinger and Christoph Kreutz 16 On-Line and At-Line LC-NMR and Related Micro-NMR Methods 379 Nadine Bohni, Emerson F. Queiroz and Jean-Luc Wolfender 17 New Developments of Laser Desorption Ionization Mass Spectrometry in Plant Analysis 411 Andreas Schinkovitz, Denis Seraphin and Pascal Richomme VOLUME II List of Contributors xi Preface xvii In Memoriam Andrew Marston xix Part Three: Strategies for Selective Classes of Compounds 425 18 Analysis of Plant Oligo- and Polysaccharides 427 Wolfgang Blaschek 19 Analytical Strategies for Multipurpose Studies of a Plant Volatile Fraction 447 Cecilia Cagliero, Barbara Sgorbini, Chiara Cordero, Erica Liberto, Carlo Bicchi and Patrizia Rubiolo 20 Strategies for Lipid Analysis 467 Irina A. Guschina and John L. Harwood 21 HPLC Analysis of Alkaloids 485 Bras Heleno de Oliveira 22 Identification and Characterization of Hydroxycinnamates of Six Galium Species from the Rubiaceae Family 505 Rakesh Jaiswal, Marius F. Matei, Sagar Deshpande and Nikolai Kuhnert 23 Identification and Characterization of Trimeric Proanthocyanidins of Two Members of the Rhododendron Genus (Ericaceae) by Liquid Chromatography Multi-Stage Mass Spectrometry 525 Rakesh Jaiswal, Mohamed G. E. Karar and Nikolai Kuhnert 24 Strategies in the Analysis of Flavonoids 543 Celestino Santos-Buelga and Ana M. Gonzalez-Paramas 25 Coumarins - Analytical and Preparative Techniques 569 Krystyna Skalicka-Wözniak and Kazimierz G¿owniak 26 Naphthoquinones and Anthraquinones: Chemical, Analytical, and Biological Overview 595 Nahed El-Najjar, Hala Gali-Muhtasib, Pia Vuorela, Arto Urtti and Heikki Vuorela 27 Xanthones from Marine-Derived Microorganisms: Isolation, Structure Elucidation, and Biological Activities 611 Madalena M. M. Pinto, Raquel A. P. Castanheiro and Anake Kijjoa 28 Sesquiterpenes and Other Terpenoids 633 Eirini Kouloura, Job Tchoumtchoua, Maria Halabalaki and Alexios-Leandros Skaltsounis 29 Analysis of Plant Saponins 687 Justyna Krzyzanowska, Mariusz Kowalczyk and Wieslaw Oleszek 30 Cardiotonic Glycosides 709 Liselotte Krenn 31 Plant Steroids: Occurrence, Biological Significance, and Their Analysis 727 G. M. Kamal B. Gunaherath and A. A. Leslie Gunatilaka 32 Chemical Analysis of Bryophytes 753 Yoshinori Asakawa, Agnieszka Ludwiczuk and Masao Toyota 33 Cyclotide Analysis 807 Susan E. Northfield, Aaron G. Poth, Charlotte D'Souza and David J. Craik VOLUME III List of Contributors xi Preface xvii In Memoriam Andrew Marston xix Part Four: Biological Analysis 825 34 Phenotyping 827 Qiaosheng Guo and Zaibiao Zhu 35 Identification of Medicinal Plants Using DNA Barcoding 843 Xiaohui Pang and Shilin Chen 36 Transcriptome Analysis of Medicinal Plants with Next-Generation Sequencing Technologies 847 Shilin Chen and Hongmei Luo 37 Microarray 859 Chang Liu, Haimei Chen, Jianqin Li and Xiaolan Xu 38 Small RNAs 875 Shanfa Lu 39 Metabolomics 885 Jan Schripsema and Denise Dagnino 40 Proteomics and Its Research Techniques in Plants 903 Liming Yang, Haibin Xu and Shilin Chen 41 Multivariate Data Analysis 915 Bieke Dejaegher Part Five: Drugs from Plants 947 42 In Silico-Guided Strategies for the Discovery and Rationalization of Bioactive Natural Products 949 Petra H. Pfisterer, Daniela Schuster, Judith M. Rollinger and Hermann Stuppner 43 Innovative Strategies in the Search for Bioactive Plant Constituents 967 Emerson F. Queiroz and Jean-Luc Wolfender 44 High Throughput Screening of Vegetal Natural Substances 987 Bruno David and Frederic Ausseil 45 Mycotoxins Contamination in Food: Alternative Plant Preservatives, Legislation, and Detection Methods 1011 Monica R. Zuzarte, Ana P. Martins, Maria J. Goncalves and Lígia R. Salgueiro 46 Quality Assessment of Herbal Drugs and Medicinal Plant Products 1039 Iqbal Ahmad, Mohd Sajjad Ahmad Khan and Swaranjit Singh Cameotra Part Six: Conclusion and Perspectives 1057 47 Conclusion and Perspectives 1059 Index 1061
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