Darcy C Burns, William F Reynolds

Optimizing NMR Methods for Structure Elucidation (eBook, ePUB)

Characterizing Natural Products and Other Organic Compounds

• Format: ePub

Produktbeschreibung

This book is aimed at informing organic chemists and natural products chemists on the use of NMR for structure elucidation to enable them to ensure they yield the most reliable possible data in the minimum possible time. It covers the latest pulse sequences, acquisition and processing methods, practical areas not covered in most texts e.g. detailed consideration of the relative advantages and disadvantages of different pulse sequences, choosing acquisition and processing parameters to get the best possible data in the least possible time, pitfalls to avoid and how to minimize the risks of getting wrong structures. Useful in industrial, pharma or research environments, this reference book is for anyone involved with organic chemistry research and, in particular, natural products research requiring advice for getting the best results from the NMR facilities.

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Produktdetails

• Verlag: RSC
• Seitenzahl: 238
• Erscheinungstermin: 26. September 2018
• Englisch
• ISBN-13: 9781788015356
• Artikelnr.: 56827345

Inhaltsangabe

Introduction
Basics of the NMR Experiment
Pulsed Fourier Transform NMR
The NMR Spectrometer
Acquiring 1H and13C Spectra
One-dimensional Pulse Sequences
Two-Dimensional NMR Basics
Two-dimensional Homonuclear Spectroscopy
Heteronuclear Shift Correlation Sequences
Sample Dereplication and Data Archiving
Using Combinations of 2D NMR Spectral Data for Ab Initio Structure Elucidation of Natural Products and Other Unknown Organic Compounds
Avoiding Getting the Wrong Structure
What Does the Future Hold for Small Molecule Structure Elucidation by NMR