Pj Goodhew

Specimen Preparation for Transmission Electron Microscopy of Materials (eBook, ePUB)

• Format: ePub

Produktbeschreibung

Details the essential practical steps which must precede microscopy. Methods for preparing sheet or disc specimens and final thinning techniques are described with reference to practical problems.

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Produktdetails

• Verlag: Taylor & Francis
• Seitenzahl: 46
• Erscheinungstermin: 25. November 2020
• Englisch
• ISBN-13: 9781000142761
• Artikelnr.: 60544929

Autorenporträt

Department of Materials Science and Engineering, University of Surrey.

Inhaltsangabe

1 The specimen: what we are trying to achieve
1.1 Thinking ahead
1.2 The ideal specimen
2 Initial preparation of sheet or disc
2.1 Cutting the slice
2.2 Preparing flat faces
2.3 Chemical thinning solutions
2.4 Making a disc
3 Final thinning
3.1 Electropolishing
3.2 Thinning a sheet: the window technique
3.3 Thinning a disc: the automatic jet polisher
3.4 Recipes for electropolishing
3.5 Ion beam thinning
3.6 Other final thinning techniques
3.7 Thinning specific regions of a sample
3.8 Thin foils from just beneath the surface
3.9 Cross
sections perpendicular to the original surface
4 Replicas
4.1 The role of the replica in modern microscopy
4.2 The extraction replica
5 Mounting and storing specimens
5.1 Grids
5.2 Disc specimens
5.3 Thinned foils
5.4 Support films
5.5 Specimen storage
Appendix. Materials and suppliers
References
Index.