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Spectroscopy and Characterization of Nanomaterials and Novel Materials Comprehensive overview of nanomaterial characterization methods and applications from leading researchers in the field In Spectroscopy and Characterization of Nanomaterials and Novel Materials: Experiments, Modeling, Simulations, and Applications, the editor Prabhakar Misra and a team of renowned contributors deliver a practical and up-to-date exploration of the characterization and applications of nanomaterials and other novel materials, including quantum materials and metal clusters. The contributions cover…mehr
Spectroscopy and Characterization of Nanomaterials and Novel Materials
Comprehensive overview of nanomaterial characterization methods and applications from leading researchers in the field
In Spectroscopy and Characterization of Nanomaterials and Novel Materials: Experiments, Modeling, Simulations, and Applications, the editor Prabhakar Misra and a team of renowned contributors deliver a practical and up-to-date exploration of the characterization and applications of nanomaterials and other novel materials, including quantum materials and metal clusters. The contributions cover spectroscopic characterization methods for obtaining accurate information on optical, electronic, magnetic, and transport properties of nanomaterials.
The book reviews nanomaterial characterization methods with proven relevance to academic and industry research and development teams, and modern methods for the computation of nanomaterials' structure and properties - including machine-learning approaches - are also explored. Readers will also find descriptions of nanomaterial applications in energy research, optoelectronics, and space science, as well as:
A thorough introduction to spectroscopy and characterization of graphitic nanomaterials and metal oxides
Comprehensive explorations of simulations of gas separation by adsorption and recent advances in Weyl semimetals and axion insulators
Practical discussions of the chemical functionalization of carbon nanotubes and applications to sensors
In-depth examinations of micro-Raman imaging of planetary analogs
Perfect for physicists, materials scientists, analytical chemists, organic and polymer chemists, and electrical engineers, Spectroscopy and Characterization of Nanomaterials and Novel Materials: Experiments, Modeling, Simulations, and Applications will also earn a place in the libraries of sensor developers and computational physicists and modelers.
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Inhaltsangabe
Preface xix About the Editor xxvii
Part I Spectroscopy and Characterization 1
1 Spectroscopic Characterization of Graphitic Nanomaterials and Metal Oxides for Gas Sensing 3 Olasunbo Farinre, Hawazin Alghamdi, and Prabhakar Misra 1.1 Introduction and Overview 3 1.1.1 Graphitic Nanomaterials 3 1.1.1.1 Synthesis of Graphitic Nanomaterials 5 1.1.2 Metal Oxides 8 1.2 Spectroscopic Characterization of Graphitic Nanomaterials and Metal Oxides 9 1.2.1 Graphitic Nanomaterials 9 1.2.1.1 Characterization of Carbon Nanotubes (CNTs) 10 1.2.1.2 Characterization of Graphene and Graphene Nanoplatelets (GnPs) 11 1.2.2 Characterization of Tin Dioxide (SnO2) 12 1.3 Graphitic Nanomaterials and Metal Oxide-Based Gas Sensors 19 1.3.1 Fabrication of Graphitic Nanomaterials-Based Gas Sensors 19 1.3.1.1 Carbon Nanotube (CNT)-Based Gas Sensors 19 1.3.1.2 Graphene and Graphene Nanoplatelet (GnP)-Based Gas Sensors 20 1.3.2 Fabrication of Metal Oxide-Based Gas Sensors 21 1.3.2.1 Tin Dioxide (SnO2)-Based Gas Sensors 23 1.4 Conclusions and Future Work 24 Acknowledgments 26 References 26
2 Low-dimensional Carbon Nanomaterials: Synthesis, Properties, and Applications Related to Heat Transfer, Energy Harvesting, and Energy Storage 33 Mahesh Vaka, Tejaswini Rama Bangalore Ramakrishna, Khalid Mohammad, and Rashmi Walvekar 2.1 Introduction 33 2.2 Synthesis and Properties of Low-dimensional Carbon Nanomaterials 35 2.2.1 Zero-dimensional Carbon Nanomaterials (0-DCNs) 35 2.2.1.1 Fullerene 35 2.2.1.2 Carbon-encapsulated Metal Nanoparticles 35 2.2.1.3 Nanodiamond 37 2.2.2 Onion-like Carbons 38 2.2.3 One-dimensional Carbon Nanomaterials 39 2.2.3.1 Carbon Nanotube 39 2.2.3.2 Carbon Fibers 39 2.2.4 Two-dimensional Carbon Nanomaterials 40 2.3 Applications 42 2.3.1 Hydrogen Storage 42 2.3.2 Solar Cells 43 2.3.3 Thermal Energy Storage 44 2.3.4 Energy Conversion 45 2.4 Conclusions 46 References 46
3 Mesoscale Spin Glass Dynamics 55 Samaresh Guchhait 3.1 Introduction 55 3.2 What Is a Spin Glass? 56 3.2.1 Spin Glass and Its Correlation Length 57 3.2.2 Mesoscale Spin Glass Dynamics 60 3.3 Summary 64 Acknowledgments 64 References 64
4 Raman Spectroscopy Characterization of Mechanical and Structural Properties of Epitaxial Graphene 67 Amira Ben Gouider Trabelsi, Feodor V. Kusmartsev, Anna Kusmartseva, and Fatemah Homoud Alkallas 4.1 Introduction 67 4.2 Epitaxial Graphene Mechanical Properties Investigation 68 4.2.1 Optical Location of Epitaxial Graphene Layers 68 4.2.2 Raman Location of Mechanical Properties Changes 71 4.2.2.1 Graphene 2D Mode 71 4.2.2.2 G Mode Investigation 74 4.2.2.3 Strain Percentage 76 4.3 Raman Polarization Study 77 4.3.1 Size Domain of Graphene Layer 77 4.3.2 Polarization Study 78 4.4 Conclusions 80 Acknowledgments 80 References 80
5 Raman Spectroscopy Studies of III?V Type II Superlattices 83 Henan Liu and Yong Zhang 5.1 Introduction 83 5.2 Raman Study on InAs/GaSb SL 84 5.2.1 Analysis on (001) Scattering Geometry 85 5.2.2 Analysis on (110) Scattering Geometry 86 5.3 Raman Study on InAs/InAs1-xSbx SL 90 5.3.1 Raman Results for the Constituent Bulks and InAs1-xSbx Alloys 90 5.3.2 Analysis on (001) Scattering Geometry for the SLs 93 5.3.3 Analysis on (110) Scattering for the SLs 95 5.4 A Comparison Among the InAs/InAs1-xSbx, InAs/GaSb, and GaAs/AlAs SLs 97 5.5 Conclusion 98 References 98
6 Dissecting the Molecular Properties of Nanoscale Materials Using Nuclear Magnetic Resonance Spectroscopy 101 Nipanshu Agarwal and Krishna Mohan Poluri 6.1 Introduction to Nanomaterials 101 6.2 Techniques Used for Characterization of Nanomaterials 104 6.3 Nuclear Magnetic Resonance (NMR) Spectroscopy 105 6.3.1 Prin
1 Spectroscopic Characterization of Graphitic Nanomaterials and Metal Oxides for Gas Sensing 3 Olasunbo Farinre, Hawazin Alghamdi, and Prabhakar Misra 1.1 Introduction and Overview 3 1.1.1 Graphitic Nanomaterials 3 1.1.1.1 Synthesis of Graphitic Nanomaterials 5 1.1.2 Metal Oxides 8 1.2 Spectroscopic Characterization of Graphitic Nanomaterials and Metal Oxides 9 1.2.1 Graphitic Nanomaterials 9 1.2.1.1 Characterization of Carbon Nanotubes (CNTs) 10 1.2.1.2 Characterization of Graphene and Graphene Nanoplatelets (GnPs) 11 1.2.2 Characterization of Tin Dioxide (SnO2) 12 1.3 Graphitic Nanomaterials and Metal Oxide-Based Gas Sensors 19 1.3.1 Fabrication of Graphitic Nanomaterials-Based Gas Sensors 19 1.3.1.1 Carbon Nanotube (CNT)-Based Gas Sensors 19 1.3.1.2 Graphene and Graphene Nanoplatelet (GnP)-Based Gas Sensors 20 1.3.2 Fabrication of Metal Oxide-Based Gas Sensors 21 1.3.2.1 Tin Dioxide (SnO2)-Based Gas Sensors 23 1.4 Conclusions and Future Work 24 Acknowledgments 26 References 26
2 Low-dimensional Carbon Nanomaterials: Synthesis, Properties, and Applications Related to Heat Transfer, Energy Harvesting, and Energy Storage 33 Mahesh Vaka, Tejaswini Rama Bangalore Ramakrishna, Khalid Mohammad, and Rashmi Walvekar 2.1 Introduction 33 2.2 Synthesis and Properties of Low-dimensional Carbon Nanomaterials 35 2.2.1 Zero-dimensional Carbon Nanomaterials (0-DCNs) 35 2.2.1.1 Fullerene 35 2.2.1.2 Carbon-encapsulated Metal Nanoparticles 35 2.2.1.3 Nanodiamond 37 2.2.2 Onion-like Carbons 38 2.2.3 One-dimensional Carbon Nanomaterials 39 2.2.3.1 Carbon Nanotube 39 2.2.3.2 Carbon Fibers 39 2.2.4 Two-dimensional Carbon Nanomaterials 40 2.3 Applications 42 2.3.1 Hydrogen Storage 42 2.3.2 Solar Cells 43 2.3.3 Thermal Energy Storage 44 2.3.4 Energy Conversion 45 2.4 Conclusions 46 References 46
3 Mesoscale Spin Glass Dynamics 55 Samaresh Guchhait 3.1 Introduction 55 3.2 What Is a Spin Glass? 56 3.2.1 Spin Glass and Its Correlation Length 57 3.2.2 Mesoscale Spin Glass Dynamics 60 3.3 Summary 64 Acknowledgments 64 References 64
4 Raman Spectroscopy Characterization of Mechanical and Structural Properties of Epitaxial Graphene 67 Amira Ben Gouider Trabelsi, Feodor V. Kusmartsev, Anna Kusmartseva, and Fatemah Homoud Alkallas 4.1 Introduction 67 4.2 Epitaxial Graphene Mechanical Properties Investigation 68 4.2.1 Optical Location of Epitaxial Graphene Layers 68 4.2.2 Raman Location of Mechanical Properties Changes 71 4.2.2.1 Graphene 2D Mode 71 4.2.2.2 G Mode Investigation 74 4.2.2.3 Strain Percentage 76 4.3 Raman Polarization Study 77 4.3.1 Size Domain of Graphene Layer 77 4.3.2 Polarization Study 78 4.4 Conclusions 80 Acknowledgments 80 References 80
5 Raman Spectroscopy Studies of III?V Type II Superlattices 83 Henan Liu and Yong Zhang 5.1 Introduction 83 5.2 Raman Study on InAs/GaSb SL 84 5.2.1 Analysis on (001) Scattering Geometry 85 5.2.2 Analysis on (110) Scattering Geometry 86 5.3 Raman Study on InAs/InAs1-xSbx SL 90 5.3.1 Raman Results for the Constituent Bulks and InAs1-xSbx Alloys 90 5.3.2 Analysis on (001) Scattering Geometry for the SLs 93 5.3.3 Analysis on (110) Scattering for the SLs 95 5.4 A Comparison Among the InAs/InAs1-xSbx, InAs/GaSb, and GaAs/AlAs SLs 97 5.5 Conclusion 98 References 98
6 Dissecting the Molecular Properties of Nanoscale Materials Using Nuclear Magnetic Resonance Spectroscopy 101 Nipanshu Agarwal and Krishna Mohan Poluri 6.1 Introduction to Nanomaterials 101 6.2 Techniques Used for Characterization of Nanomaterials 104 6.3 Nuclear Magnetic Resonance (NMR) Spectroscopy 105 6.3.1 Prin
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