The Synthesis Of Metal Complexes With Macrocyclic Glyoxime Ether - Karapinar, Emin
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In this work, by the reaction of four different chloroglyoximes with 4 -Amminobenzo[15-Crown-5] in absolute ethanol, eight of new macrocylic glyoxime ether compounds and their Ni(II), Co(II) and Cu(II) complexes have been synthesized. For this, firstly chlorophenylglyoxime, p-tolylchloroglyoxime, p-chlorophenyl chloroglyoxime and 4 -biphenylchloroglyoxime were synthesized according to previously reported literatures. Then novel glyoxime derivatives with macrocyclic glyoxime ethers by the reactions between these compounds with 4 -amminobenzo[15-crown-5] were obtained. The complexes of these…mehr

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Produktbeschreibung
In this work, by the reaction of four different chloroglyoximes with 4 -Amminobenzo[15-Crown-5] in absolute ethanol, eight of new macrocylic glyoxime ether compounds and their Ni(II), Co(II) and Cu(II) complexes have been synthesized. For this, firstly chlorophenylglyoxime, p-tolylchloroglyoxime, p-chlorophenyl chloroglyoxime and 4 -biphenylchloroglyoxime were synthesized according to previously reported literatures. Then novel glyoxime derivatives with macrocyclic glyoxime ethers by the reactions between these compounds with 4 -amminobenzo[15-crown-5] were obtained. The complexes of these ligands with metal chlorid salts have been formed. Finally, the UV-VIS, IR, AAS and 1H NMR spectroscopic properties of these compounds were investigated and clarified by the help of the results of elemental analyses and the spectroscopic methods. The content of this book is based on an experimental study for my Ph.D thesis submitted to Selcuk University, Konya, Turkey in 2002.
Autorenporträt
Emin Karapinar was born in 1973 in Ankara. He graduated from Selcuk University with B.Sc. degree in Chemistry Department in 1994. He received his M.Sc. degree from Pamukkale University in 1996. He completed his Ph.D studies in 2002 at the Selcuk University.He has been working as a faculty member at Pamukkale University since 1994.