Joseph D. Menczel, R. Bruce Prime
Thermal Analysis of Polymers
Herausgeber: Menczel, Joseph D; Prime, R Bruce
Joseph D. Menczel, R. Bruce Prime
Thermal Analysis of Polymers
Herausgeber: Menczel, Joseph D; Prime, R Bruce
- Gebundenes Buch
- Merkliste
- Auf die Merkliste
- Bewerten Bewerten
- Teilen
- Produkt teilen
- Produkterinnerung
- Produkterinnerung
Presents a solid introduction to thermal analysis, methods, instrumentation, calibration, and application along with the necessary theoretical background. Useful to chemists, physicists, materials scientists, and engineers who are new to thermal analysis techniques, and to existing users of thermal analysis who wish expand their experience to new techniques and applications Topics covered include Differential Scanning Calorimetry and Differential Thermal Analysis (DSC/DTA), Thermogravimetry, Thermomechanical Analysis and Dilatometry, Dynamic Mechanical Analysis, Micro-Thermal Analysis, Hot…mehr
Andere Kunden interessierten sich auch für
- WileyCharacterization and Analysis of Polymers476,99 €
- Thermal Analysis of Polymeric Materials199,00 €
- Stepan PodzimekLight Scattering, Size Exclusion Chromatography and Asymmetric Flow Field Flow Fractionation138,99 €
- Ali MorsaliFunctional Metal-Organic Frameworks207,99 €
- Tomas TorresOrganic Nanomaterials213,99 €
- Barbara H. StuartPolymer Analysis113,99 €
- Polymers for Biomedicine288,99 €
-
-
-
Presents a solid introduction to thermal analysis, methods, instrumentation, calibration, and application along with the necessary theoretical background.
Useful to chemists, physicists, materials scientists, and engineers who are new to thermal analysis techniques, and to existing users of thermal analysis who wish expand their experience to new techniques and applications
Topics covered include Differential Scanning Calorimetry and Differential Thermal Analysis (DSC/DTA), Thermogravimetry, Thermomechanical Analysis and Dilatometry, Dynamic Mechanical Analysis, Micro-Thermal Analysis, Hot Stage Microscopy, and Instrumentation.
Written by experts in the various areas of thermal analysis
Relevant and detailed experiments and examples follow each chapter.
Hinweis: Dieser Artikel kann nur an eine deutsche Lieferadresse ausgeliefert werden.
Useful to chemists, physicists, materials scientists, and engineers who are new to thermal analysis techniques, and to existing users of thermal analysis who wish expand their experience to new techniques and applications
Topics covered include Differential Scanning Calorimetry and Differential Thermal Analysis (DSC/DTA), Thermogravimetry, Thermomechanical Analysis and Dilatometry, Dynamic Mechanical Analysis, Micro-Thermal Analysis, Hot Stage Microscopy, and Instrumentation.
Written by experts in the various areas of thermal analysis
Relevant and detailed experiments and examples follow each chapter.
Hinweis: Dieser Artikel kann nur an eine deutsche Lieferadresse ausgeliefert werden.
Produktdetails
- Produktdetails
- Verlag: Wiley & Sons
- 1. Auflage
- Seitenzahl: 704
- Erscheinungstermin: 1. April 2009
- Englisch
- Abmessung: 240mm x 161mm x 42mm
- Gewicht: 1078g
- ISBN-13: 9780471769170
- ISBN-10: 0471769177
- Artikelnr.: 23875774
- Verlag: Wiley & Sons
- 1. Auflage
- Seitenzahl: 704
- Erscheinungstermin: 1. April 2009
- Englisch
- Abmessung: 240mm x 161mm x 42mm
- Gewicht: 1078g
- ISBN-13: 9780471769170
- ISBN-10: 0471769177
- Artikelnr.: 23875774
Joseph D. Menczel, PhD, a recognized expert in thermal analysis of polymers with some thirty years of industrial and academic experience, is Assistant Technical Director at Alcon Laboratories. He has researched more than 120 polymeric systems in which he studied calibration of DSCs, glass transition, nucleation, crystallization, melting, stability, mechanical and micro-mechanical properties of polymers, and polymer-water interactions. Dr. Menczel holds six patents and is the author of seventy scholarly papers. He is the author of two chapters in the bookThermal Characterization of Polymeric Materials. In conducting DSC experiments, Dr. Menczel found a crystal/amorphous interface in semicrystalline polymers, which later became known as the rigid amorphous phase. He is also credited with developing the temperature calibration of DSCs for cooling experiments. R. Bruce Prime, PhD, is a consultant to industry and government and a recognized authority on the cure and properties of cross-linked polymer systems. During his thirty-year career with IBM, he led teams responsible for developing and implementing polymer applications for printer and information storage technologies. He holds four patents and is the author of more than fifty technical papers and the chapter on thermosets in Thermal Characterization of Polymeric Materials. Dr. Prime is a Fellow of SPE and NATAS and was the 1989 recipient of the Mettler-Toledo Award in Thermal Analysis. He maintains the Web site www.primethermosets.com.
Chapter I: Introduction (Joseph D. Menczel, R. Bruce Prime and Patrick K.
Gallagher). Chapter II: Differential Scanning Calorimetry (Joseph D.
Menczel, Lawrence H. Judovits, R. Bruce Prime, Harvey E. Bair, Mike
Reading, and Steven Swier). 1. Introduction. 2. Elements of Thermodynamics
in DSC. 3. The Basics of Differential Scanning Calorimetry. 4. Purity
Determination of Low Molecular Mass Compounds by DSC. 5. Calibration of
Differential Scanning Calorimeters. 6. The Measurement of Heat Capacity. 7.
Phase Transitions in Amorphous and Crystalline Polymers. 8. DSC of Fibers.
9. Films. 10. Thermosets. 11. Differential Photocalorimetry (DPC). 12. Fast
Scan DSC. 13. Modulated Temperature Differential Scanning Calorimetry
(MTDSC). 14. How to Perform DSC Measurements . 15. Instrumentation.
References. Chapter III: Thermogravimetric Analysis (TGA) (R. Bruce Prime,
Harvey E. Bair, Sergey Vyazovkin, Patrick K. Gallagher, and Alan Riga). 1.
Introduction. 2. Background Principles and Measurement Modes. 3.
Calibration and Reference Materials. 4. Measurements and Analyses. 5.
Kinetics. 6. Selected Applications. 7. Instrumentation. Appendix.
References. Chapter IV: Thermomechanical Analysis (TMA) and
Thermodilitometry (TD) (Harvey E. Bair, Ali E. Akinay, Joseph D. Menczel,
R. Bruce Prime, and Michael Jaffe). 1. Introduction. 2. Principles and
Theory. 3. Instrumental. 4. Calibration. 5. How to Perform a TMA
Experiment. 6. Key Applications. 7. Selected Industrial Applications.
Appendix. References. Chapter V: Dynamic Mechanical Analysis (DMA) (Richard
P. Chartoff, Joseph D. Menczel, and Steven H. Dillman). 1. Introduction. 2.
Characterization of viscoelastic behavior. 3. Applications of dynamic
mechanical analysis. 4. Examples of DMA characterization for
thermoplastics. 5. Characteristics of fibers and thin films. 6. DMA
characterization of cross-linked polymers. 7. Practical Aspects of
Conducting DMA Experiments. 8. Commercial DMA Instrumentation. Appendix.
References. Chapter VI: Dielectric Analysis (DEA) (Aglaia Vassilikou-Dova
and Ioannis M. Kalogeras). 1. Introduction. 2. Theory and background of
dielectric analysis. 3. Dielectric techniques. 4. Performing dielectric
experiments. 5. Typical measurements on poly(methyl methacrylate) (PMMA).
6. Dielectric Analysis of Thermoplastics. 7. Dielectric Analysis of
Thermosets. 8. Instrumentation. Appendix. References. Chapter VII: Micro
and Nano Scale Local Thermal Analysis (Valeriy V. Gorbunov, David Grandy,
Mike Reading, and Vladimir V. Tsukruk). 1. Introduction. 2. The Atomic
Force Microscope. 3. Scanning Thermal Microscopy. 4. Thermal Probe Design
and Spatial Resolution. 5. Measuring Thermal Conductivity and Thermal
Force-Distance Curves. 6. Local Thermal Analysis. 7. Performing a
Micro/Nano Thermal Analysis Experiment. 8. Examples of Micro/Nano Thermal
Analysis Applications. 9. Overview of Local Thermal Analysis. References.
Gallagher). Chapter II: Differential Scanning Calorimetry (Joseph D.
Menczel, Lawrence H. Judovits, R. Bruce Prime, Harvey E. Bair, Mike
Reading, and Steven Swier). 1. Introduction. 2. Elements of Thermodynamics
in DSC. 3. The Basics of Differential Scanning Calorimetry. 4. Purity
Determination of Low Molecular Mass Compounds by DSC. 5. Calibration of
Differential Scanning Calorimeters. 6. The Measurement of Heat Capacity. 7.
Phase Transitions in Amorphous and Crystalline Polymers. 8. DSC of Fibers.
9. Films. 10. Thermosets. 11. Differential Photocalorimetry (DPC). 12. Fast
Scan DSC. 13. Modulated Temperature Differential Scanning Calorimetry
(MTDSC). 14. How to Perform DSC Measurements . 15. Instrumentation.
References. Chapter III: Thermogravimetric Analysis (TGA) (R. Bruce Prime,
Harvey E. Bair, Sergey Vyazovkin, Patrick K. Gallagher, and Alan Riga). 1.
Introduction. 2. Background Principles and Measurement Modes. 3.
Calibration and Reference Materials. 4. Measurements and Analyses. 5.
Kinetics. 6. Selected Applications. 7. Instrumentation. Appendix.
References. Chapter IV: Thermomechanical Analysis (TMA) and
Thermodilitometry (TD) (Harvey E. Bair, Ali E. Akinay, Joseph D. Menczel,
R. Bruce Prime, and Michael Jaffe). 1. Introduction. 2. Principles and
Theory. 3. Instrumental. 4. Calibration. 5. How to Perform a TMA
Experiment. 6. Key Applications. 7. Selected Industrial Applications.
Appendix. References. Chapter V: Dynamic Mechanical Analysis (DMA) (Richard
P. Chartoff, Joseph D. Menczel, and Steven H. Dillman). 1. Introduction. 2.
Characterization of viscoelastic behavior. 3. Applications of dynamic
mechanical analysis. 4. Examples of DMA characterization for
thermoplastics. 5. Characteristics of fibers and thin films. 6. DMA
characterization of cross-linked polymers. 7. Practical Aspects of
Conducting DMA Experiments. 8. Commercial DMA Instrumentation. Appendix.
References. Chapter VI: Dielectric Analysis (DEA) (Aglaia Vassilikou-Dova
and Ioannis M. Kalogeras). 1. Introduction. 2. Theory and background of
dielectric analysis. 3. Dielectric techniques. 4. Performing dielectric
experiments. 5. Typical measurements on poly(methyl methacrylate) (PMMA).
6. Dielectric Analysis of Thermoplastics. 7. Dielectric Analysis of
Thermosets. 8. Instrumentation. Appendix. References. Chapter VII: Micro
and Nano Scale Local Thermal Analysis (Valeriy V. Gorbunov, David Grandy,
Mike Reading, and Vladimir V. Tsukruk). 1. Introduction. 2. The Atomic
Force Microscope. 3. Scanning Thermal Microscopy. 4. Thermal Probe Design
and Spatial Resolution. 5. Measuring Thermal Conductivity and Thermal
Force-Distance Curves. 6. Local Thermal Analysis. 7. Performing a
Micro/Nano Thermal Analysis Experiment. 8. Examples of Micro/Nano Thermal
Analysis Applications. 9. Overview of Local Thermal Analysis. References.
Chapter I: Introduction (Joseph D. Menczel, R. Bruce Prime and Patrick K.
Gallagher). Chapter II: Differential Scanning Calorimetry (Joseph D.
Menczel, Lawrence H. Judovits, R. Bruce Prime, Harvey E. Bair, Mike
Reading, and Steven Swier). 1. Introduction. 2. Elements of Thermodynamics
in DSC. 3. The Basics of Differential Scanning Calorimetry. 4. Purity
Determination of Low Molecular Mass Compounds by DSC. 5. Calibration of
Differential Scanning Calorimeters. 6. The Measurement of Heat Capacity. 7.
Phase Transitions in Amorphous and Crystalline Polymers. 8. DSC of Fibers.
9. Films. 10. Thermosets. 11. Differential Photocalorimetry (DPC). 12. Fast
Scan DSC. 13. Modulated Temperature Differential Scanning Calorimetry
(MTDSC). 14. How to Perform DSC Measurements . 15. Instrumentation.
References. Chapter III: Thermogravimetric Analysis (TGA) (R. Bruce Prime,
Harvey E. Bair, Sergey Vyazovkin, Patrick K. Gallagher, and Alan Riga). 1.
Introduction. 2. Background Principles and Measurement Modes. 3.
Calibration and Reference Materials. 4. Measurements and Analyses. 5.
Kinetics. 6. Selected Applications. 7. Instrumentation. Appendix.
References. Chapter IV: Thermomechanical Analysis (TMA) and
Thermodilitometry (TD) (Harvey E. Bair, Ali E. Akinay, Joseph D. Menczel,
R. Bruce Prime, and Michael Jaffe). 1. Introduction. 2. Principles and
Theory. 3. Instrumental. 4. Calibration. 5. How to Perform a TMA
Experiment. 6. Key Applications. 7. Selected Industrial Applications.
Appendix. References. Chapter V: Dynamic Mechanical Analysis (DMA) (Richard
P. Chartoff, Joseph D. Menczel, and Steven H. Dillman). 1. Introduction. 2.
Characterization of viscoelastic behavior. 3. Applications of dynamic
mechanical analysis. 4. Examples of DMA characterization for
thermoplastics. 5. Characteristics of fibers and thin films. 6. DMA
characterization of cross-linked polymers. 7. Practical Aspects of
Conducting DMA Experiments. 8. Commercial DMA Instrumentation. Appendix.
References. Chapter VI: Dielectric Analysis (DEA) (Aglaia Vassilikou-Dova
and Ioannis M. Kalogeras). 1. Introduction. 2. Theory and background of
dielectric analysis. 3. Dielectric techniques. 4. Performing dielectric
experiments. 5. Typical measurements on poly(methyl methacrylate) (PMMA).
6. Dielectric Analysis of Thermoplastics. 7. Dielectric Analysis of
Thermosets. 8. Instrumentation. Appendix. References. Chapter VII: Micro
and Nano Scale Local Thermal Analysis (Valeriy V. Gorbunov, David Grandy,
Mike Reading, and Vladimir V. Tsukruk). 1. Introduction. 2. The Atomic
Force Microscope. 3. Scanning Thermal Microscopy. 4. Thermal Probe Design
and Spatial Resolution. 5. Measuring Thermal Conductivity and Thermal
Force-Distance Curves. 6. Local Thermal Analysis. 7. Performing a
Micro/Nano Thermal Analysis Experiment. 8. Examples of Micro/Nano Thermal
Analysis Applications. 9. Overview of Local Thermal Analysis. References.
Gallagher). Chapter II: Differential Scanning Calorimetry (Joseph D.
Menczel, Lawrence H. Judovits, R. Bruce Prime, Harvey E. Bair, Mike
Reading, and Steven Swier). 1. Introduction. 2. Elements of Thermodynamics
in DSC. 3. The Basics of Differential Scanning Calorimetry. 4. Purity
Determination of Low Molecular Mass Compounds by DSC. 5. Calibration of
Differential Scanning Calorimeters. 6. The Measurement of Heat Capacity. 7.
Phase Transitions in Amorphous and Crystalline Polymers. 8. DSC of Fibers.
9. Films. 10. Thermosets. 11. Differential Photocalorimetry (DPC). 12. Fast
Scan DSC. 13. Modulated Temperature Differential Scanning Calorimetry
(MTDSC). 14. How to Perform DSC Measurements . 15. Instrumentation.
References. Chapter III: Thermogravimetric Analysis (TGA) (R. Bruce Prime,
Harvey E. Bair, Sergey Vyazovkin, Patrick K. Gallagher, and Alan Riga). 1.
Introduction. 2. Background Principles and Measurement Modes. 3.
Calibration and Reference Materials. 4. Measurements and Analyses. 5.
Kinetics. 6. Selected Applications. 7. Instrumentation. Appendix.
References. Chapter IV: Thermomechanical Analysis (TMA) and
Thermodilitometry (TD) (Harvey E. Bair, Ali E. Akinay, Joseph D. Menczel,
R. Bruce Prime, and Michael Jaffe). 1. Introduction. 2. Principles and
Theory. 3. Instrumental. 4. Calibration. 5. How to Perform a TMA
Experiment. 6. Key Applications. 7. Selected Industrial Applications.
Appendix. References. Chapter V: Dynamic Mechanical Analysis (DMA) (Richard
P. Chartoff, Joseph D. Menczel, and Steven H. Dillman). 1. Introduction. 2.
Characterization of viscoelastic behavior. 3. Applications of dynamic
mechanical analysis. 4. Examples of DMA characterization for
thermoplastics. 5. Characteristics of fibers and thin films. 6. DMA
characterization of cross-linked polymers. 7. Practical Aspects of
Conducting DMA Experiments. 8. Commercial DMA Instrumentation. Appendix.
References. Chapter VI: Dielectric Analysis (DEA) (Aglaia Vassilikou-Dova
and Ioannis M. Kalogeras). 1. Introduction. 2. Theory and background of
dielectric analysis. 3. Dielectric techniques. 4. Performing dielectric
experiments. 5. Typical measurements on poly(methyl methacrylate) (PMMA).
6. Dielectric Analysis of Thermoplastics. 7. Dielectric Analysis of
Thermosets. 8. Instrumentation. Appendix. References. Chapter VII: Micro
and Nano Scale Local Thermal Analysis (Valeriy V. Gorbunov, David Grandy,
Mike Reading, and Vladimir V. Tsukruk). 1. Introduction. 2. The Atomic
Force Microscope. 3. Scanning Thermal Microscopy. 4. Thermal Probe Design
and Spatial Resolution. 5. Measuring Thermal Conductivity and Thermal
Force-Distance Curves. 6. Local Thermal Analysis. 7. Performing a
Micro/Nano Thermal Analysis Experiment. 8. Examples of Micro/Nano Thermal
Analysis Applications. 9. Overview of Local Thermal Analysis. References.