Quantitative Chemical Analysis by Mass Spectrometry provides a serious introduction to the subject of mass spectrometry, providing the reader with the tools and information to be well prepared to perform such demanding work in a real life laboratory. Fundiert, verständlich, anwendungsorientiert: Im Lehrbuchstil verfasst, führt das Werk so in die Massenspektrometrie ein, dass seine Leser nach gründlicher Lektüre in der Lage sind, die hier vorgestellten Techniken - insbesondere moderne Massenspektrometer - im Labor einzusetzen.
Quantitative Chemical Analysis by Mass Spectrometry provides a serious introduction to the subject of mass spectrometry, providing the reader with the tools and information to be well prepared to perform such demanding work in a real life laboratory.Fundiert, verständlich, anwendungsorientiert: Im Lehrbuchstil verfasst, führt das Werk so in die Massenspektrometrie ein, dass seine Leser nach gründlicher Lektüre in der Lage sind, die hier vorgestellten Techniken - insbesondere moderne Massenspektrometer - im Labor einzusetzen.Hinweis: Dieser Artikel kann nur an eine deutsche Lieferadresse ausgeliefert werden.
Professor Robert K Boyd, National Research Council, Institute for National Measurement Standards, Ottawa, Canada Robert Boyd obtained his B Sc and Ph D from St Andrews University. In 1962 he took a post-doctoral fellow position at NRC followed by periods at the University of Toronto & University of Guelph. In 1986 he re-joined the NRC, and since that time has served as adjunct professor at Dalhousie University (1992-2001). Since 2001 he has been Researcher Emeritus at the NRC in Ottawa. Professor Boyd has published over 160 research papers, four book chapters & 10 NRC Technical reports. In 1002 he received the Maxxam Award for Analytical Chemistry and in 2003 the Queen Elizabeth II Gold Jubilee Medal. He is currently Chair of the Science Advisory Board for the Genome Prarie project on enabling technologies for proteomics. And a member of the NSERC Committee for Scientific & Technical review of ISTC proposals. He was an editor for Rapid Communications in Mass Spectrometry from 1990 - 1997 and from 1997 - 2005 was the journal's Editor-in-Chief. Dr Robert A Bethem, senior VP of the Bioanalytical Group at Alta Analytical Laboratory, CA, USA and Professor Dwight Matthews of the University of Vermont, USA
Inhaltsangabe
Preface. Acknowledgements. 1 Measurement, Dimensions and Units. 2 Tools of the Trade I. The Classical Tools. 3 Tools of the Trade II. Theory of Chromatography. Appendix 3.1 Derivation of the Plate Theory Equation for Chromatographic Elution. Appendix 3.2 Transformation of the Plate Theory Elution Equation from Poisson to Gaussian Form. Appendix 3.3 A Brief Introduction to Snyder's Theory of Gradient Elution. List of Symbols Used in Chapter 3. 4 Tools of the Trade III. Separation Practicalities. Appendix 4.1 Responses of Chromatographic Detectors: Concentration vs Mass-Flux Dependence. 5 Tools of the Trade IV. Interfaces and Ion Sources for Chromatography-Mass Spectrometry. 6 Tools of the Trade V. Mass Analyzers for Quantitation: Separation of Ions by m/z Values. Appendix 6.1 Interaction of Electric and Magnetic Fields with Charged Particles. Appendix 6.2 Leak Detection. Appendix 6.3 List of Symbols Used in Chapter 6. 7 Tools of the Trade VI. Ion Detection and Data Processing. 8 Tools of the Trade VII: Statistics of Calibration, Measurement and Sampling. Appendix 8.1 A Brief Statistics Glossary. Appendix 8.2 Symbols Used in Discussion of Calibration Methods. 9 Method Development and Fitness for Purpose. 10 Method Validation and Sample Analysis in a Controlled Laboratory Environment. 11 Examples from the Literature. Epilog. References. Index.
Preface. Acknowledgements. 1 Measurement, Dimensions and Units. 2 Tools of the Trade I. The Classical Tools. 3 Tools of the Trade II. Theory of Chromatography. Appendix 3.1 Derivation of the Plate Theory Equation for Chromatographic Elution. Appendix 3.2 Transformation of the Plate Theory Elution Equation from Poisson to Gaussian Form. Appendix 3.3 A Brief Introduction to Snyder's Theory of Gradient Elution. List of Symbols Used in Chapter 3. 4 Tools of the Trade III. Separation Practicalities. Appendix 4.1 Responses of Chromatographic Detectors: Concentration vs Mass-Flux Dependence. 5 Tools of the Trade IV. Interfaces and Ion Sources for Chromatography-Mass Spectrometry. 6 Tools of the Trade V. Mass Analyzers for Quantitation: Separation of Ions by m/z Values. Appendix 6.1 Interaction of Electric and Magnetic Fields with Charged Particles. Appendix 6.2 Leak Detection. Appendix 6.3 List of Symbols Used in Chapter 6. 7 Tools of the Trade VI. Ion Detection and Data Processing. 8 Tools of the Trade VII: Statistics of Calibration, Measurement and Sampling. Appendix 8.1 A Brief Statistics Glossary. Appendix 8.2 Symbols Used in Discussion of Calibration Methods. 9 Method Development and Fitness for Purpose. 10 Method Validation and Sample Analysis in a Controlled Laboratory Environment. 11 Examples from the Literature. Epilog. References. Index.
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