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The present work reports the design of experimental work to be executed for establishing approximate generalized empirical model for Processing time, Weight of briquette at outlet, Power, resistive torque, temperature rise, Percentage of moisture content, Percentage of Ash content and calorific value of briquettes during Briquette manufacturing Process on the basis of experimentation data chosen, using methodology of engineering experimentation. This research also includes the design and manufacture of process of Briquette along with theory of experimentation. It also includes formulation of mathematical model and its sensitivity analysis, reliability, optimization and limiting values. Designing of experimental setup for measurement of power, current drawn, processing resistive torque, temperature and time required for each processing operations using specially designed circuits is also mentioned in this work.